Enantiospecific synthesis of [7R, 6S, 5S, 4R]-triacetoxy-(-)-goniotriol

G.S.C.Srikanth; Urlam Murali Krishna; Girish K.Trivedi

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Enantiospecific synthesis of [7R, 6S, 5S, 4R]-triacetoxy-(-)-goniotriol

机译：[7R，6S，5S，4R]-三乙酰氧基-（-）-goniotriol的对映体合成

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摘要

A short and efficient synthesis of [7R,6S,5S,4R]-triacetoxy-(-)-goniotriol starting form D-glucose is described. A sequence of ring closing metathesis (RCM) followed by a PCC oxidation was used to construct the core six-membered alpha, beta-unsaturated lactone moiety.

机译：描述了由D-葡萄糖起始的[7R，6S，5S，4R]-三乙酰氧基-（-）-goniotriol的短而有效的合成。一系列闭环复分解（RCM），然后进行PCC氧化，用于构建核心的六元α，β-不饱和内酯部分。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2002年第31期|共3页
作者
G.S.C.Srikanth; Urlam Murali Krishna; Girish K.Trivedi;
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正文语种 eng
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styryllactones; goniotriol; ring closing metathesis; PCC oxidation;

机译：苯乙烯基内酯;角酚三醇;闭环复分解;PCC氧化;

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专利

1. Enantiospecific synthesis of [7R, 6S, 5S, 4R]-triacetoxy-(-)-goniotriol [J] . G.S.C.Srikanth, Urlam Murali Krishna, Girish K.Trivedi Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2002,第31期

机译：[7R，6S，5S，4R]-三乙酰氧基-（-）-goniotriol的对映体合成
2. Syn-selective michael addition of amines to bis-enones: synthesis of 1,3,4,7-tetrasubstituted (4R,5S,6S,7R)-hexahydro-5,6-dihydroxy-2H-1,3-diazepin-2-ones [J] . Erwin P.Schreiner, Arno Pruckner The Journal of Organic Chemistry . 1997,第16期

机译：将胺同选择性迈克尔加成至双烯酮：合成1,3,4,7-四取代（4R，5S，6S，7R）-六氢-5,6-二羟基-2H-1,3-二氮杂-2 -那些
3. Synthesis of (4R,12S,15S,16S,19R,20R,34S)-Muricatetrocin and (4R,12S,15S,16S,19R,20R,34S)-Muricatertrocin,Two Potent Inhibitors of Mitochondrial Complex I [J] . Baurle Stefan, Peters Ulf, Friedrich Thorsten, European journal of organic chemistry . 2000,第12aJuna期

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4. Design and Analysis of a New 7R Single-Loop Mechanism with 4R, 6R and 7R Operation Modes [C] . Xiuyun He, Xianwen Kong, Guangbo Hao, ASME/IFToMM International Conference on Reconfigurable Mechanisms and Robots . 2016

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5. Total synthesis of nominal 4S,7R, 11S,14R Cyclocinamide B and analysis of three stereoisomers of Cyclocinamide A. [D] . Curzon, Stephanie Maureen Stepp. 2012

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6. 5-{(2S3R4S5S6R)-34-Dihydroxy-6-hydroxymethyl-3-(2S3R4R5R6S)-345-trihydroxy-6-methyltetrahydropyran-2-yloxytetrahydropyran-2-yloxy}-7-hydroxy-2-(4-hydroxyphenyl)chromen-4-one monohydrate [O] . Yuzhen Chen, Airong Wang, Haiyan Gao, 2008

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7. (1R,4R,6S,7R)-5,5-Dibromo-1,4,8,8-tetramethyltricyclo[5.4.1.04,6]dodecan-12-one [O] . Mohamed Zaki, Ahmed Benharref, Jean-Claude Daran, 2014

机译：（1R，4R，6s，7R）-5,5-二溴1,4,8,8-tetramethyltricyclo [5.4.1.04,6]十二烷-12-酮

Enantiospecific synthesis of [7R, 6S, 5S, 4R]-triacetoxy-(-)-goniotriol

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