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A novel approach to prepare silver chloride nanoparticles grown on the surface of PAN nanofibre via electrospinning combined with gas–solid reaction

机译:通过电纺结合气固反应制备在PAN纳米纤维表面生长的氯化银纳米颗粒的新方法

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摘要

Well-defined silver chloride nanoparticles grown on the surface of PAN nanofibre were synthesized by electrospinning technology combined with gas–solid reaction. This method can avoid the possibility of the waste of raw material as well as enhance the usage rate of AgNO3. The PAN nanofibre can be recycled easily. X-ray powder diffraction (XRD) shows the presence of crystal AgCl, X-ray photoelectron spectroscopy (XPS) confirm that there are chemical bonds and interaction between the surface modified PAN nanofibre and Ag ions. This will be propitious to prevent nanoparticles from aggregation. Field-emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM) gave the direct evidence that AgCl nanoparticles have been dispersed on the surface of PAN nanofibre homogeneously.
机译:通过电纺丝技术结合气固反应合成了在PAN纳米纤维表面上生长的明确定义的氯化银纳米颗粒。该方法可以避免原料浪费的可能性,并提高了AgNO 3的利用率。 PAN纳米纤维可以轻松回收。 X射线粉末衍射(XRD)表明存在AgCl晶体,X射线光电子能谱(XPS)证实表面改性的PAN纳米纤维与Ag离子之间存在化学键和相互作用。这将有利于防止纳米颗粒聚集。场发射扫描电子显微镜(FESEM)和透射电子显微镜(TEM)直接证明了AgCl纳米颗粒已经均匀地分散在PAN纳米纤维的表面上。

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