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Fluid filtration and rheological properties of nanoparticle additive and intercalated clay hybrid bentonite drilling fluids

机译:纳米颗粒添加剂和插层粘土杂土膨润土钻井液的流体过滤和流变特性

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The fluid filtration and rheological properties of low solid content (LSC) bentonite fluids containing iron-oxide (Fe2O3) nanoparticle (NP) additives and two different NP intercalated clay hybrids, iron-oxide clay hybrid (ICH) and aluminosilicate clay hybrid (ASCH), under both low-temperature low-pressure (LTLP: 25 degrees C, 6.9 bar) and high-temperature high-pressure (HTHP: 200 degrees C, 70 bar) conditions are investigated. The viscosity of each fluid was measured under LTLP and HTHP conditions using a pressurized and heated rotational viscometer. The LTLP and HTHP fluid filtrate volumes were measured in accordance to American Petroleum Institute standards. The addition of ICH and ASCH into bentonite solutions reduced both LTLP and HTHP fluid loss as much as 37% and 47% as compared to the control, under the respective conditions. The pure addition of 0.5 wt% 3 and 30 nm Fe2O3 NP increased the LTLP fluid filtration as much as 14% as compared to the control. However, this addition of Fe2O3 NP decreased the HTHP fluid filtrate volumes as much as 28% as compared to the control. It was found that the addition of clay hybrids reduced LTLP and HTHP fluid loss due to a restructured mode of clay platelet interaction attributed to a modification in surface charge as demonstrated by zeta potential measurements and scanning electron microscope images. (C) 2015 Elsevier B.V. All rights reserved.
机译:包含氧化铁(Fe2O3)纳米颗粒(NP)添加剂和两种不同的NP插层粘土杂化体,铁氧化物粘土杂化体(ICH)和硅铝酸盐粘土杂化体(ASCH)的低固含量(LSC)膨润土流体的流体过滤和流变特性分别在低温低压(LTLP:25摄氏度,6.9巴)和高温高压(HTHP:200摄氏度,70巴)条件下进行研究。使用加压和加热的旋转粘度计在LTLP和HTHP条件下测量每种流体的粘度。 LTLP和HTHP流体滤液的体积根据美国石油学会的标准进行测量。在相应的条件下,与对照相比,在膨润土溶液中添加ICH和ASCH可将LTLP和HTHP的流体损失分别降低37%和47%。与对照组相比,纯添加0.5 wt%3和30 nm Fe2O3 NP可使LTLP流体过滤提高14%。然而,与对照相比,这种Fe 2 O 3 NP降低了HTHP流体滤液的体积多达28%。发现通过zeta电势测量和扫描电子显微镜图像证明,由于粘土血小板相互作用的重构模式归因于表面电荷的改变,粘土杂化物的加入减少了LTLP和HTHP的流体损失。 (C)2015 Elsevier B.V.保留所有权利。

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