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Helium bubble distributions in a nanostructured ferritic alloy

机译:纳米结构铁素体合金中的氦气气泡分布

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A 14YWT nanostructured ferritic alloy (NFA) was implanted with He + ions to fluences of 6.75 × 10~(21) He m~(-2) at 400 °C in order to simulate the effects of high He concentrations produced in advanced fission and future fusion reactors at an accelerated timescale. The He bubble size distributions associated with specific microstructural features were characterized by a combination of transmission electron microscopy and atom probe tomography. Helium bubbles were observed on grain boundaries, dislocations, and on the surfaces of nanoclusters and larger Ti(N,C) precipitates. A polydisperse distribution of bubble sizes was observed in the ferrite matrix. With the exception of He bubbles on dislocations, bubbles were observed to increase in size with increasing fluence. The combined TEM and APT data indicates that ~4.4% of the bubbles are located on coarse precipitates, ~12.2% at dislocations, ~14.4% at grain boundaries, and ~48.6% on nanoclusters, and the remainder as isolated bubbles in the ferrite matrix. The abundances of these different trapping sites, especially the nanoclusters, might reduce the availability and mobility of He, and possibly the susceptibility of these alloys to He embrittlement.
机译:在400°C下向Hey离子注入浓度为6.75×10〜(21)He m〜(-2)的14YWT纳米铁素体合金(NFA),以模拟在高级裂变和高温下产生的高He浓度的影响。未来的聚变反应堆将以更快的速度发展。通过结合透射电子显微镜和原子探针层析成像来表征与特定微结构特征相关的He气泡尺寸分布。在晶界,位错,纳米团簇和较大的Ti(N,C)沉淀物表面观察到氦气气泡。在铁氧体基体中观察到气泡尺寸的多分散分布。除位错上的He气泡外,观察到气泡随着通量的增加而增大。 TEM和APT的综合数据表明,约有4.4%的气泡位于粗大的析出物上,位错处的气泡为〜12.2%,晶界处的气泡为〜14.4%,纳米团簇中的气泡为〜48.6%,其余的为铁素体基体中的孤立气泡。 。这些不同的俘获位点(尤其是纳米团簇)的丰度可能会降低He的可用性和迁移率,并可能降低这些合金对He脆化的敏感性。

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