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Growth and Characterization of Electroplated NiO Coatings

机译:电镀NiO涂层的生长和表征

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摘要

Thin films of NiO have been prepared using potentiostatic electrodeposition technique from an aqueous electrolytic bath containing NiSO4. Deposited films have been characterized using x-ray diffraction, scanning electron microscopy and energy dispersive analysis by x-rays. X-ray diffraction patterns showed that the prepared films possess polycrystalline nature with face centered cubic structure. Surface morphology and film composition showed that films with better stoichiometry and smooth surface are obtained at optimized growth condition. Optical absorption analysis showed that the prepared films possess direct band gap value around 3.46 eV.
机译:NiO薄膜已使用恒电位电沉积技术从含NiSO4的水性电解浴中制备。已经使用X射线衍射,扫描电子显微镜和通过X射线的能量色散分析来表征沉积的膜。 X射线衍射图表明,所制备的薄膜具有面心立方结构的多晶性质。表面形貌和膜组成表明,在优化的生长条件下可获得具有更好的化学计量和光滑表面的膜。光吸收分析表明,所制备的薄膜具有直接的带隙值,约为3.46eV。

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