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Effect of Synthetic Temperature on the Dispersion Stability of Gold Nanocolloid Produced via Electrical Explosion of Wire

机译:合成温度对金属丝电爆炸产生金纳米胶体分散稳定性的影响

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摘要

In this study, gold nanocolloid was produced via the electrical explosion of wire in water, for the purpose of medical treatment. Thus, the use of other additives was avoided to stabilize the gold nanocolloid. The temperature of the water that was to be used for explosion was changed, and its effect on the stability of the gold nanocolloid was investigated. The synthetic temperature was varied from ice temperature to 80℃. The morphology and particle size were studied using a transmission electron microscope. The UV-Vis spectra confirmed the formation of gold nanoparticles in the water. The stability of the gold nanocolloid was estimated using the zeta-potential and Turbis-can methods. The results showed that the synthetic temperature affected the stability of the gold nanocolloid. The TEM images of the gold nanoparticles prepared at low temperatures (0 and 20℃) have several big particles. But, when the synthetic temperature was increased to 80℃, most of the nanoparticles formed a spherical shape, without neck connection. Better stability was obtained in the gold nanocolloid sample prepared at a higher temperature. The gold nanocolloid that was synthesized at 80℃ was stable for more than three months, with small sedimentation.
机译:在这项研究中,金纳米胶体是通过电线在水中的电爆炸产生的,用于医疗目的。因此,避免了使用其他添加剂来稳定金纳米胶体。改变了用于爆炸的水的温度,并研究了其对金纳米胶体稳定性的影响。合成温度从冰温度变化到80℃。使用透射电子显微镜研究形态和粒径。 UV-Vis光谱证实了水中金纳米颗粒的形成。金纳米胶体的稳定性是使用zeta电位和Turbis-can方法估算的。结果表明,合成温度影响金纳米胶体的稳定性。在低温(0和20℃)下制备的金纳米颗粒的TEM图像有几个大颗粒。但是,当合成温度升至80℃时,大多数纳米颗粒形成球形,没有颈连接。在较高温度下制备的金纳米胶体样品具有较好的稳定性。在80℃下合成的金纳米胶体在超过三个月的时间内稳定下来,并且沉降很小。

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