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首页> 外文期刊>Journal of nanoparticle research: An interdisciplinary forum for nanoscale science and technology >Preparation and characterization of Ag/ZnO composites via a simple hydrothermal route
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Preparation and characterization of Ag/ZnO composites via a simple hydrothermal route

机译:通过简单的水热法制备和表征Ag / ZnO复合材料

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Silver/zinc oxide (Ag/ZnO) composites were fabricated by a facile one-pot synthesis method under hydrothermal conditions. By choosing glucose as the reductant, metal Ag was fabricated from Ag_20 with the growth of the crystalline ZnO. Structure measurements revealed that obtained Ag/ZnO composites comprised wurtzite ZnO and face-centered cubic structure of nanosized Ag, which uniformly distributed in the composites. Moreover, the morphology of the ZnO was varied regularly with the formation of Ag nanoparticles from flower-like to rod-like and finally returned to flower-like. The optical properties of UV—Vis and surface-enhanced Raman scattering spectra of the composites as well as effects of the dimension of metal Ag fabricated during the prior period of reaction on the morphology of ZnO were discussed.
机译:在水热条件下,通过简便的一锅法合成银/氧化锌(Ag / ZnO)复合材料。通过选择葡萄糖作为还原剂,随着晶体ZnO的生长,由Ag_20制备金属Ag。结构测量表明,获得的Ag / ZnO复合材料包含纤锌矿ZnO和纳米级Ag的面心立方结构,它们均匀分布在复合物中。此外,ZnO的形貌随着Ag纳米颗粒的形成从花状到棒状而有规律地变化,并最终恢复为花状。讨论了复合材料的紫外可见光谱和表面增强拉曼散射光谱,以及反应前期制备的金属银的尺寸对ZnO形貌的影响。

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