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Taking piezoelectric microsystems from the laboratory to production

机译:将压电微系统从实验室运用于生产

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Reliable integration of piezoelectric thin films into silicon-based microsystems on an industrial scale is a key enabling technology for a wide range of future products. However, current knowledge in the field is mostly limited to the conditions and scale of academic laboratories. Thus, knowledge on performance, reliability and reproducibility of the films and methods at industrial level is scarce. The present study intends to contribute to the development of reliable technology for integration of piezoelectric thin films into MEMS on an industrial scale. A test wafer design that contained more than 500 multimorph cantilevers, bridges and membranes in the size range between 50 and 1,500 μm was developed. The active piezoelectric material was a ~2 μm thin film of lead zirconate titanate (PZT) deposited by a state-of-the-art chemical solution deposition (CSD) procedure. Automated measurements of C(V) and dielectric dissipation factor at 1 kHz were made on more than 200 devices at various locations across the wafer surface. The obtained standard deviations were 4.5 and 11% for the permittivity and dissipation factor, respectively. Values for the transverse piezoelectric charge coefficient, e{sub}(31,f), of up to -15.1 C/m{sup}2 were observed. Fatigue tests with a 5 kHz signal applied to a typical cantilever at ± 25 V led to less than 10% reduction of the remanent polarisation after 2 × 10{sup}7 bipolar cycles. Cantilever out-of-plane deflection at zero field measured after poling was less than 1.1% for a typical 800 μm cantilever.
机译:在工业规模上将压电薄膜可靠地集成到基于硅的微系统中,是广泛应用未来产品的关键技术。但是,当前在该领域的知识大多限于学术实验室的条件和规模。因此,在工业水平上缺乏关于膜和方法的性能,可靠性和再现性的知识。本研究旨在为在工业规模上将压电薄膜集成到MEMS中的可靠技术的发展做出贡献。开发了一种测试晶圆设计,其中包含500多个多晶型悬臂,桥和膜,尺寸范围在50至1,500μm之间。活性压电材料是通过最先进的化学溶液沉积(CSD)程序沉积的〜2μm钛酸锆钛酸铅(PZT)薄膜。在整个晶片表面上不同位置的200多种设备上,进行了1 kHz时C(V)和介电损耗因子的自动测量。介电常数和耗散系数的标准偏差分别为4.5%和11%。观察到横向压电电荷系数e {sub}(31,f)的值高达-15.1 C / m {sup} 2。将5 kHz信号施加在±25 V的典型悬臂上的疲劳测试导致在2×10 7个双极循环后剩余极化的减少幅度不到10%。对于典型的800μm悬臂,极化后在零场处测得的悬臂平面外偏转小于1.1%。

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