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The Effect of Resin Matrix Composition on Mechanical Properties of E-glass Fiber-Reinforced Composite for Dental Use

机译:树脂基体组成对牙科用电子玻璃纤维增​​强复合材料力学性能的影响

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摘要

The effects of resin matrix composition including bis-phenol-A-diglycidyl dimethacrylate (bis-GMA)-methyl methacrylate (MMA) based or urethane dimethacrylate (UEDMA)-triethylene glycol dimethacrylate (TEGDMA) based composition and storage conditions on the mechanical properties of E-glass fiberreinforced composites (FRCs) were studied. Three experimental groups ('Exper 1', 'Exper 2', 'Exper 3') with differing UEDMA to TEGDMA ratio in the matrix together with a control group ('Control') based on bis-GMA-MMA resin matrix were prepared by light-curing. The storage conditions for each group were dry storage at room temperature for 24 h and 30- and 60-day immersion in deionized (DI) water at 37°C, which further divided each group into three subgroups. For all the four composition groups, mechanical properties including hardness, flexural strength and modulus in both three-point and four-point bendings were tested (n = 6), together with water sorption and solubility study (n = 6) and fracture site scanning with a scanning electron microscope (SEM). The experimental specimens were relatively streng and stiff in three-point bending compared to previous research. The same specimens in three-point bending had a lower flexural modulus and fractured at higher flexural stress than in four-point bending. According to the SEM images after fracture, some resin matrix was still bound to the uber surface, showing cohesive-interfacial fracture type and relatively stable matrix-fiber adhesion. According to comprehensive analysis, the control group showed superior mechanical Performance in most of the tests.
机译:包括双酚A-二甲基丙烯酸二缩水甘油酯(bis-GMA)-甲基丙烯酸甲酯(MMA)或氨基甲酸酯二甲基丙烯酸酯(UEDMA)-三乙二醇二甲基丙烯酸酯(TEGDMA)的树脂基体组成和储存条件对其力学性能的影响研究了电子玻璃纤维增​​强复合材料(FRC)。制备了三个实验组('Exper 1','Exper 2','Exper 3')和基于bis-GMA-MMA树脂基质的对照组('Control'),它们在基质中具有不同的UEDMA与TEGDMA比率。光固化。每组的储存条件为在室温下干燥保存24小时,然后在37°C的去离子(DI)水中浸泡30天和60天,这进一步将每组分为三个亚组。对于所有四个成分组,均测试了机械特性,包括三点和四点弯曲的硬度,弯曲强度和模量(n = 6),以及吸水和溶解度研究(n = 6)以及断裂部位扫描用扫描电子显微镜(SEM)。与以前的研究相比,实验样品在三点弯曲中相对坚硬。与四点弯曲相比,相同的三点弯曲试样具有较低的弯曲模量,并且在较高的弯曲应力下破裂。根据断裂后的SEM图像,一些树脂基体仍然结合在uber表面上,表现出内聚界面断裂类型和相对稳定的基体-纤维粘合。根据综合分析,对照组在大多数测试中均显示出优异的机械性能。

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