Transformations of alkyl (5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetates into 5-heteroaryl-3-oxo-2-phenyl-3,5-dihydro-2H-pyrazolo[4,3-c]pyridine-7-carboxylates

David Bevk; Renata Jakse; Jurij Svete; Amalija Golobic; Lujbo Golic; Branko Stanovnik

首页> 外文期刊>Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry >Transformations of alkyl (5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetates into 5-heteroaryl-3-oxo-2-phenyl-3,5-dihydro-2H-pyrazolo[4,3-c]pyridine-7-carboxylates

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Transformations of alkyl (5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetates into 5-heteroaryl-3-oxo-2-phenyl-3,5-dihydro-2H-pyrazolo[4,3-c]pyridine-7-carboxylates

机译：（5-氧代-1-苯基-4,5-二氢-1H-吡唑-3-基）乙酸烷基酯转化成5-杂芳基-3-氧代-2-苯基-3,5-二氢-2H-吡唑并[5]。 4,3-c]吡啶-7-羧酸盐

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Alkyl [(Z)-4-dimethylaminomethylidene-5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl]acetate (4) was transformed with N- and C-nucleophiles into alkyl [4-(subsituted amino)methylidene-4,5-dihydro-1H-pyrazol-3-yl]acetates (7) and alkyl (4-heteroarylmethylidene-4,5-dihydro-1H-pyrazol-3-yl)acetates (8),respectively.Compounds (7) cyclize by heating with DMFDMA in DMF into 2H-pyrazolo[4,3-c]pyridine-7-carboxylates (9).

机译：[（Z）-4-二甲基氨基亚甲基-5-氧代-1-苯基-4,5-二氢-1H-吡唑-3-基]乙酸烷基酯（4）用N-和C-亲核试剂转化为烷基[4- （取代的氨基）亚甲基-4,5-二氢-1H-吡唑-3-基]乙酸酯（7）和（4-杂芳基亚甲基-4,5-二氢-1H-吡唑-3-基）乙酸酯（8），化合物（7）通过在DMF中与DMFDMA加热而环化成2H-吡唑并[4,3-c]吡啶-7-羧酸盐（9）。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2003年第1期|共27页
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David Bevk; Renata Jakse; Jurij Svete; Amalija Golobic; Lujbo Golic; Branko Stanovnik;
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1. Transformations of alkyl (5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetates into 5-heteroaryl-3-oxo-2-phenyl-3,5-dihydro-2H-pyrazolo[4,3-c]pyridine-7-carboxylates [J] . David Bevk, Renata Jakse, Jurij Svete, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2003,第1期

机译：（5-氧代-1-苯基-4,5-二氢-1H-吡唑-3-基）乙酸烷基酯转化成5-杂芳基-3-氧代-2-苯基-3,5-二氢-2H-吡唑并[5]。 4,3-c]吡啶-7-羧酸盐
2. 4-Functionally Substituted 3-Heterylpyrazoles:XVIII.*Intramolecular Cyclization of N-[3-(2-Chlorophenyl)-4-pyrazolyl]methylamine and Its N-Alkyl Derivatives into 4,5-Dihydro-2H-pyrazolo[4,3-c]quinolines [J] . M.K.Bratenko, O.I.Panimarchuk, V.A.Chornous Russian Journal of Organic Chemistry . 2007,第8期

机译：N- [3-（2-氯苯基）-4-吡唑基]甲胺及其N-烷基衍生物的分子内环化成4,5-二氢-2H-吡唑并[4,3]的四官能取代的3-杂基吡唑：XVIII。 -c]喹啉
3. Intramolecular Cycloaddition Approach to Fused Pyrazoles: Access to 4,5-Dihydro-2H-pyrazolo[4,3-c]quinolines, 2,8-Dihydroindeno[2,1-c]pyrazoles, and 4,5-Dihydro-2H-benzo[e]indazoles [J] . Moumita Jash, Bimolendu Das, Suparna Sen, Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2018,第7期

机译：融合吡唑的分子内环加成方法：获得4,5-二氢-2H-吡唑[4,3-C]喹啉，2,8-二氢吲哚[2,1-C]吡唑，4,5-二氢-2H- Benzo [E] Indazoles
4. 3-C A SEARCH FOR AN INTERACTIVE FLAME RETARDANT SYSTEM FOR ETHYLENE-VINYL ACETATE [C] . Edward D.Weil, Menachem Lewin, Dattatray Rao, the Conference on Recent Advances in Flame Retardancy of Polymeric Materials . 2004

机译：3-C A搜索用于乙烯 - 乙酸乙烯乙烯酯的相互作用的阻燃系统
5. Chemical and microbiological transformations induced in oilfield produced water by amendment with nitrate as a souring control measure: Investigation of sulfur cycling, effects of co-amendment with acetate and phosphate, and evaluation of storage protocols. [D] . Hulecki, Jordan Christopher. 2009

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6. Nonenzymatic and enzymatic hydrolysis of alkyl halides: A theoretical study of the SN2 reactions of acetate and hydroxide ions with alkyl chlorides [O] . Andreas H. Maulitz, Felice C. Lightstone, Ya-Jun Zheng, 1997

机译：烷基卤的非酶水解和酶水解：乙酸和乙酸的SN2反应的理论研究。烷基氯化物产生氢氧根离子
7. ALKYL–ALKYL COUPLING OF LITHIUM ALKYLALUMINATES AND ALKYL–ALLYL CROSS-COUPLING OF THE ALUMINATES WITH ALLYLIC HALIDES BY THE USE OF COPPER (II) ACETATE: AN APPLICATION OF THE CATALYTIC HYDROALUMINATION OF OLEFINS TO ORGANIC SYNTHESIS [O] . Kakuzo Isagawa, Manabu Ohige, Kimio Tatsumi, 1978

机译：锂烷基烷基烷基偶联硅酸铝与铝酸盐的烷基铝与烯丙基锂的交联：乙酸酯的应用：烯烃催化水中催化与有机合成的应用

Transformations of alkyl (5-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-3-yl)acetates into 5-heteroaryl-3-oxo-2-phenyl-3,5-dihydro-2H-pyrazolo[4,3-c]pyridine-7-carboxylates

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