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Influence of annealing and deformation on optical properties of ultra precision diamond turned and anodized 6060 aluminium alloy

机译:退火和变形对超精密金刚石车削和阳极氧化6060铝合金光学性能的影响

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摘要

Influence of cold forging, and subsequent heat treatment and diamond turning on optical quality of anodized film on 6060 (AlMgSi) alloy was investigated and compared with microstructural changes. Heat treatment of the samples was carried out either prior to forging, post-forging, or both. The surface of the forged material was then diamond turned to a mirror like finish. The diamond turned samples were subsequently anodized in a sulphuric acid bath. The microstructure of the samples was analysed using optical microscopy (LOM), scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX). Colour/brightness measurements were carried out using CIE Lab system. An optical method was used to measure the thickness of the oxide film and roughness of the surface was measured before and after anodizing using stylus, a mechanical instrument, and bidirectional reflection distribution function (BRDF), an optical instrument. Results indicated that the post-forging heat treatment had a great influence on the appearance of the anodized layer, which was also a function of the deformation introduced prior to heat treatment. The effect was assumed to be attributed to the change in microstructure, especially the distribution and the amount of the intermetallic particles such as elemental Si and Mg2Si. Roughness of the oxide film was also found to be a function of the heat treatment and deformation condition.
机译:研究了冷锻,随后的热处理和金刚石车削对6060(AlMgSi)合金上阳极氧化膜光学质量的影响,并与显微组织变化进行了比较。样品的热处理是在锻造之前,锻造之后或两者同时进行的。然后,将锻造材料的表面用金刚石磨成镜面状的表面。随后将金刚石车削的样品在硫酸浴中进行阳极氧化。使用光学显微镜(LOM),扫描电子显微镜(SEM)和能量色散X射线光谱(EDX)分析样品的微观结构。使用CIE Lab系统进行颜色/亮度测量。在使用触笔,机械仪器和双向反射分布函数(BRDF),光学仪器进行阳极氧化之前和之后,使用光学方法测量氧化膜的厚度并测量表面的粗糙度。结果表明,锻后热处理对阳极氧化层的外观有很大的影响,这也是热处理之前引入的变形的函数。认为该影响归因于微观结构的变化,特别是金属间颗粒如元素Si和Mg2Si的分布和数量。还发现氧化膜的粗糙度是热处理和变形条件的函数。

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