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Assessment of microstructural and mechanical properties of HVOF sprayed WC-based cermet coatings for a roller cylinder

机译:辊筒用HVOF喷涂WC基金属陶瓷涂料的显微组织和力学性能评估

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The present paper concerns an assessment of microstructural and mechanical properties of WC-based cermet coatings for a roller cylinder. With this regard, WC-based coatings were fabricated on NiAl deposited 316 L stainless steel substrates by using HVOF technique. The produced coatings were extensively analyzed with respect to X-ray diffraction (XRD), optical microscopy, image analyzer, scanning electron microscopy (SEM) including energy dispersive spectroscopy (EDS), microhardness and surface roughness. Adhesion strength of the coatings was also measured by using a scratch tester and the scratch was examined with an optical microscope. XRD study revealed that WC, W,C, W, C, Co, CoW9C, Co8W9C, Ni, NiAl, Ni3Al and FeNi phases are present in the coatings. The metallographical observations showed that all coatings had a similar coating microstructure and good contact to the substrate, highly dense structure, low oxide and porosity contents. In addition to structural and microstructural results, microhardness values of WC-Co, WC-Ni, NiAl coatings and stainless steel were measured to be 1700, 1750, 450 and 220 HV, respectively. It was found that the adhesion force value of WC-Co coating (125.9 MPa) is higher than WC-Ni coating (76.2 MPa). In order to determine wear loss, friction coefficient and wear mechanism, wear tests were performed for the WC-Co and WC-Ni coated NiAl deposited stainless steel substrates at 50 and 100 N loads under dry sliding conditions through a pin-on-plate arrangement against AISI 303 L steel counterbody. Regarding wear mechanism of the coatings, the microstructural analysis of worn surfaces was examined by SEM and EDS. It was found that the friction coefficients of WC-Co coating are higher than WC-Ni coating under 50 and 100 N loads at dry sliding conditions. In addition to this, the total wear loss of the WC-Co coating is more than WC-Ni coating on NiAl deposited stainless steel substrates. (c) 2005 Published by Elsevier B.V.
机译:本发明涉及用于辊筒的基于WC的金属陶瓷涂层的微观结构和机械性能的评估。考虑到这一点,通过使用HVOF技术,在NiAl沉积的316 L不锈钢基材上制备了WC基涂层。所产生的涂层在X射线衍射(XRD),光学显微镜,图像分析仪,扫描电子显微镜(SEM)(包括能量分散光谱(EDS)),显微硬度和表面粗糙度方面进行了广泛的分析。还通过使用划痕测试仪测量涂层的粘合强度,并用光学显微镜检查划痕。 XRD研究表明,涂层中存在WC,W,C,W,C,Co,CoW9C,Co8W9C,Ni,NiAl,Ni3Al和FeNi相。金相观察表明,所有涂层具有相似的涂层微观结构,与基材的接触良好,结构致密,氧化物和孔隙率低。除结构和微观结构结果外,WC-Co,WC-Ni,NiAl涂层和不锈钢的显微硬度值分别为1700、1750、450和220 HV。结果发现,WC-Co涂层(125.9 MPa)的附着力值高于WC-Ni涂层(76.2 MPa)。为了确定磨损损失,摩擦系数和磨损机理,在干式滑动条件下,通过销钉-板结构对WC-Co和WC-Ni涂层NiAl沉积的NiAl沉积不锈钢基底进行了磨损测试,载荷分别为50和100 N对抗AISI 303 L钢制配体。关于涂层的磨损机理,通过SEM和EDS检查了磨损表面的微观结构分析。发现在干滑条件下,在50和100 N的载荷下,WC-Co涂层的摩擦系数高于WC-Ni涂层。除此之外,在NiAl沉积的不锈钢基材上,WC-Co涂层的总磨损损失大于WC-Ni涂层。 (c)2005年由Elsevier B.V.

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