Synthesis of 1,3-dithiole-2-thiones and tetrathiafulvalenes using oligo-(1,3-dithiole-2,4,5-trithione)

G. G. Abashev; E. V. Shklyaeva

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Synthesis of 1,3-dithiole-2-thiones and tetrathiafulvalenes using oligo-(1,3-dithiole-2,4,5-trithione)

机译：用低聚-（1,3-二硫代-2,4,5-三硫酮）合成1,3-二硫代-2-硫酮和四硫富瓦烯

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摘要

Methods for the synthesis of 1,3-dithiole-2-thiones, based on [4+2] cycloaddition of the 1,3-dithiole-2,4,5-trithione oligomer to various unsaturated acyclic, carbocyclic, and heterocyclic compounds, are reviewed. Methods for the production of substituted tetrathiafulvalenes, which can be regarded as derivatives of bis(ethylenedithio)tetrathiafulvalene, from 1,3-dithiole-2-thiones synthesized by this method are described.

机译：基于1,3-二硫醇-2,4,5-三硫酮低聚物与各种不饱和无环，碳环和杂环化合物的[4 + 2]环加成反应，合成1,3-二硫代-2-硫酮的方法，被审查。描述了由通过该方法合成的1，3-二硫代-2-硫酮生产可被视为双（亚乙基二硫代）四硫富瓦烯的衍生物的取代的四硫富瓦烯的方法。

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《Chemistry of heterocyclic compounds》 |2006年第4期|共17页
作者
G. G. Abashev; E. V. Shklyaeva;
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正文语种 eng
中图分类杂环化合物;
关键词
1; 3-dithiole-2-thione; 1; 3-dithiol-2-one; 1; 3-dithiole-2; 4; 5-trithiol(ane); substituted donors; tetrathiafulvalenes; 4+2 cycloaddition;

机译：1;3-二硫代-2-硫酮;1;3-二硫代-2-酮;1;3-二硫代-2;4;5-三硫醇（烷）;取代的供体;四硫富瓦烯;[4 + 2]环加成;

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1. Synthesis of 1,3-dithiole-2-thiones and tetrathiafulvalenes using oligo-(1,3-dithiole-2,4,5-trithione) [J] . G. G. Abashev, E. V. Shklyaeva Chemistry of heterocyclic compounds . 2006,第4期

机译：用低聚-（1,3-二硫代-2,4,5-三硫酮）合成1,3-二硫代-2-硫酮和四硫富瓦烯
2. Structural and new spectroscopic properties of neutral [M(dmit)2](dmit=C_3S_5~(2-),1,3-dithiole-2-thione-4,5-dithiolate) and [M(H2timdt)2](H2timdt=H2C3N2S_3~(1-),monoanion of imidazolidine-2,4,5-trithione) complexes within the density functional appr [J] . Pina Romaniello, Francesco Lelj, Massimiliano Arca Theoretical chemistry accounts . 2007,第5a6期

机译：中性[M（dmit）2]（dmit = C_3S_5〜（2-），1,3-dithiole-2-thione-4,5-dithiolate）和[M（H2timdt）2]（H2timdt）的结构和新光谱性质= H2C3N2S_3〜（1-），咪唑烷-2,4,5-三硫酮单阴离子）配合物
3. Structural and new spectroscopic properties of neutral $[hbox{M(dmit)}_{bf 2}] (hbox{dmit} = hbox{C}_{bf 3} hbox{S}_{bf 5}^{bf 2-}$ , 1,3-dithiole-2-thione-4,5-dithiolate) and $[hbox{M}(hbox{H}_{bf 2}hbox{timdt})_{bf 2}](hbox{H}_{bf 2}hbox{timdt} = hbox{H}_{bf 2} hbox{C}_{bf 3} hbox{N}_{bf 2} hbox{S}_{bf 3}^{bf 1-}$ , monoanion of imidazolidine-2,4,5-trithione) complexes within the density functional approach [J] . Pina Romaniello, Francesco Lelj, Massimiliano Arca, Theoretical Chemistry Accounts . 2007,第5a6期

机译：中性$ [hbox {M（dmit）} _ {bf 2}]的结构和新光谱性质（hbox {dmit} = hbox {C} _ {bf 3} hbox {S} _ {bf 5} ^ {bf 2 -} $，1,3-二硫代-2-硫酮-4,5-二硫代）和$ [hbox {M}（hbox {H} _ {bf 2} hbox {timdt}）_ {bf 2}]（hbox {H} _ {bf 2} hbox {timdt} = hbox {H} _ {bf 2} hbox {C} _ {bf 3} hbox {N} _ {bf 2} hbox {S} _ {bf 3} ^密度泛函方法中的{bf 1-} $，咪唑烷2,4,5-三硫酮）络合物的单阴离子
4. Synthesis,Structures and Redox Properties of Tetrathiafulvalene and Related Bis(1,3-Dithiole)Dendrimers [C] . Martin R.Bryce, Nicolas Godbert, Christian A.Christensen PMSE Symposia . 2002

机译：Telthasfulvalene和相关双（1,3-二孔）树枝状叶片的合成，结构和氧化还原性能
5. NEW SYNTHETIC METHODS IN ORGANIC CHEMISTRY: PART I. THE SYNTHESIS AND REACTIVITY OF STERICALLY HINDERED NITRIMINES--SYNTHESIS OF IMINES. PART II. INVESTIGATIONS INTO THE SYNTHESIS AND COUPLING REACTIONS OF 1,3-DITHIOLE ANALOGS. [D] . RUSSO, JOSEPH MICHAEL. 1986

机译：有机化学的新合成方法：第一部分：空间受限的亚硝酸盐的合成和反应性—氨基酸的合成。第二部分1,3-二噻吩类似物的合成和偶联反应的研究。
6. 2,4,5-Tris(pyridin-4-yl)-4,5-dihydro-1,3-oxazole [O] . José J. Campos-Gaxiola, Herbert Höpfl, Gerardo Aguirre, 2015

机译：2,4,5-三（吡啶-4-基）-4,5-二氢-1,3-恶唑
7. In-vitro Antibacterial, Antifungal and cytotoxic activity of cobalt (II), copper (II), nickel (II) and zinc (II) complexes with furanylmethyl- and thienylmethyl-dithiolenes: 1, 3-dithiole- 2-one and 1,3-dithiole-2-thione [O] . Zahid H. Chohan, Ali U. Shaikh, Claudiu T. Supuran 2006

机译：钴（II），铜（II），铜（II），镍（II）和锌（II）配合物的体外抗菌，抗真菌和细胞毒活性，用呋喃基甲基和噻吩基甲基 - 二苯乙烯 - 1，3-二孔-2-一和1 ，3-dithiole-2-thione

Synthesis of 1,3-dithiole-2-thiones and tetrathiafulvalenes using oligo-(1,3-dithiole-2,4,5-trithione)

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