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Process optimization for PA12/MWCNT nanocomposite manufacturing by selective laser sintering

机译:选择性激光烧结制备PA12 / MWCNT纳米复合材料的工艺优化

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摘要

Nanocomposites produced through the addition of carbon nanotubes to a polymeric matrix can improve the material properties. The mobility of the polymer chains is usually affected, and this is also related to the properties. Parts produced with the free-form fabrication process using the selective laser sintering (SLS) technique can be used in different high-performance applications as they do not require expensive tools for their manufacture. A specific field of interest is the aerospace industry which is characterized by a low production volume and the need for materials with a high performance to weight ratio. In this study, the free-form fabrication by SLS of parts made from nanocomposites comprised of polyamide 12 and multiwalled carbon nanotubes (MWCNTs) was investigated. Specimens were manufactured by SLS to identify the appropriate processing parameters to achieve high mechanical properties for aerospace applications. Laser energy density was adjusted to improve the material density, flexural modulus, and stress at 10% elongation. Design of experiments was used to identify and quantify the effects of various factors on the mechanical properties. The results obtained showed that there was a limit to the amount of MWCNTs which could be mixed with the polyamide powder to improve the mechanical properties since a higher content affected the laser sintering process.
机译:通过将碳纳米管添加到聚合物基体中产生的纳米复合材料可以改善材料性能。聚合物链的迁移率通常会受到影响,这也与性能有关。使用选择性激光烧结(SLS)技术以自由形式制造工艺生产的零件可用于各种高性能应用,因为它们不需要昂贵的工具即可制造。感兴趣的特定领域是航空航天工业,其特征在于产量低并且需要具有高性能/重量比的材料。在这项研究中,研究了由SLS进行的由聚酰胺12和多壁碳纳米管(MWCNT)组成的纳米复合材料制成的零件的自由形式制造。 SLS生产的标本旨在识别适当的加工参数,以实现航空航天应用的高机械性能。调整激光能量密度以提高材料密度,弯曲模量和10%伸长率下的应力。实验设计被用来识别和量化各种因素对机械性能的影响。所获得的结果表明,可与聚酰胺粉末混合以改善机械性能的MWCNT的数量受到限制,因为较高的含量会影响激光烧结工艺。

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