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EFFECT OF THE HOMOGENIZATION PROCESS ON THE RHEOLOGICAL PROPERTIES OF FOOD EMULSIONS

机译:均质化过程对食品乳状液流变性的影响

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The aim of this study was to assess changes in rheological characteristics and droplet size distribution in emulsions studied under the influence of the one- and two-stage homogenization processes, carried out at a pressure higher than in standard industry practice. The material consisted of food emulsions of the o/w type, with an oil phase content of 9%, 12%, and 18% of mass, in a 20% solution of milk protein concentrate. The one- and two-stage homogenization processes were carried out using a ?Panda" laboratory homogenizer from GEA Niro-Soavi at the pressure of 30 MPa and 30/6 MPa at 45,0 + 0,5°C. The degree of fat despersion was determined with the microscopic method, by using computer image analysis. The flow curves of the emulsions tested weredetermined using the rheometer of the Rheostressl type with a concentric cylinder system Rotor 234 DIN 53019, at an increasing shear rate (y) ranging from 0,04 to 700 s"1. Changes in shear stress versus shear rate value O = f{y)were described using theOstwald de Waele power-law model. It was found that subjecting food emulsions to one- and two-stage homogenization pressure resulted in changes in the rheological parameters of flow curves. Droplet size depended on the percentage of oil in the emulsion and homogenization conditions. The homogenization process was followed by a significant decline of the consistency coefficient and a slight increase in the flow rate. These changes prove the effect of the homogenization process on the structure of emulsions.
机译:这项研究的目的是评估在一阶段和两阶段均质化过程的影响下,所研究乳液的流变特性和液滴尺寸分布的变化,该过程在高于标准行业惯例的压力下进行。该材料由o / w型食品乳液组成,在20%的乳蛋白浓缩液中油相含量为9%,12%和18%。使用GEA Niro-Soavi的?Panda“实验室均质器在45,0 + 0.5°C的压力下分别在30 MPa和30/6 MPa的压力下进行一阶段和两阶段均质化处理。使用显微镜方法,通过计算机图像分析确定分散液,使用流变型流变仪和同心圆筒系统Rotor 234 DIN 53019,在增加的剪切速率(y)为0的情况下,确定测试乳液的流动曲线,04至700 s“ 1。使用Ostwald de Waele幂律模型描述了剪切应力与剪切速率值O = f(y)的变化。已经发现,使食物乳液经受一阶段和两阶段均质化压力会导致流动曲线的流变参数的变化。液滴的大小取决于乳液中油的百分比和均质条件。均质过程之后,稠度系数显着下降,流速略有增加。这些变化证明了均质化过程对乳液结构的影响。

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