Synthesis of a New Thiocarbamate by the Reaction of Benzyl Thiocyanate with Camphene, Catalyzed by Heteropoly Acids

A. V. Arkhipova; K. V. Malkova; T. N. Sokolova; V. R. Kartashov

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Synthesis of a New Thiocarbamate by the Reaction of Benzyl Thiocyanate with Camphene, Catalyzed by Heteropoly Acids

机译：杂多酸催化硫氰酸苄基酯与hen烯反应合成新的硫代氨基甲酸酯

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摘要

The reaction of benzyl thiocyanate with camphene in the presence of heteropoly acids, 12-phos-photungstic and 12-silicotungstic, at 65℃ was studied. S-Benzyl (1,7,7-trimethylnorbornyl)thiocarbamate was prepared in 66% yield.

机译：研究了杂多酸，12-磷-钨和12-硅钨的存在下，硫氰酸苄酯与with烯的反应温度为65℃。制备S-苄基（1,7,7-三甲基降冰片基）硫代氨基甲酸酯，收率为66％。

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来源
《Russian journal of applied chemistry》 |2007年第1期|p.162-163|共2页
作者
A. V. Arkhipova; K. V. Malkova; T. N. Sokolova; V. R. Kartashov;
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作者单位

Nizhni Novgorod State Technical University, Nizhni Novgorod, Russia;

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正文语种 eng
中图分类应用化学;
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专利

1. Acid-catalyzed reactions of thiocyanates with camphene [J] . Arkhipova AV, Malkova KV, Sokolova TN, Kinetics and catalysis . 2008,第3期

机译：硫氰酸盐与camp烯的酸催化反应
2. Heteropoly acids catalyzed direct mannich reactions: Three-component synthesis of N-protected beta-amino ketones [J] . Wang R, Huang T, Shi L, Synlett . 2007,第14期

机译：杂多酸催化直接曼尼希反应：N保护的β-氨基酮的三组分合成
3. Synthesis of polybenzyls by Suzuki Pd-catalyzed crosscoupling of boronic acids and benzyl bromides: Model reactions and polyreactions [J] . Klarner C., Greiner A. Macromolecular rapid communications: Publishing the newsletters of the European Polymer Federation . 1998,第12期

机译：Suzuki Pd催化的硼酸和苄基溴化物的交叉偶联合成聚苄基：模型反应和多反应
4. Synthesis of Carbamates/thiocarbamates by Selenium-Catalyzed Carbonylation Reactions [C] . X.P.Zhang, Y.Yang, G.Ling, International conference on selenium in the environment and human health . 2009

机译：硒催化的羰基化反应合成氨基甲酸酯/硫代氨基甲酸酯
5. Exploration of alpha-Diazocarbonyl Compounds for Transition-Metal Catalyzed Carbon-Carbon Bond Formations. Development of Palladium-Catalyzed Stereoselective Synthesis of Trisubstituted Alkenes and the Synthesis of Quaternary alpha,alpha-Heterodiaryl Carboxylic Acids by Rhodium-Catalyzed Multi-Component Coupling Reactions. [D] . Tsoi, Yuk Tai. 2012

机译：探索用于过渡金属催化的碳-碳键形成的α-重氮羰基化合物。铑催化的多组分偶合反应在钯催化的立体选择性合成三取代的烯烃上的发展和季铵的α，α-杂二芳基羧酸的合成。
6. Palladium-Catalyzed Tandem N-Arylation/Carboamination Reactions for the Stereoselective Synthesis of N-Aryl-2-Benzyl Pyrrolidines [O] . Qifei Yang, Joshua E. Ney, John P. Wolfe -1

机译：钯催化的N-芳基-2-苄基吡咯烷的立体选择性合成N-芳基化/碳氨化反应
7. Highly Efficient One-Pot Three-Component Mannich Reaction in Water Catalyzed by Heteropoly Acids [O] . -1

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Synthesis of a New Thiocarbamate by the Reaction of Benzyl Thiocyanate with Camphene, Catalyzed by Heteropoly Acids

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