Direct oxidative coupling of amidine hydrochlorides and methylarenes: TBHP-mediated synthesis of substituted 1,3,5-triazines under metal-free conditions

Wei Guo

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Direct oxidative coupling of amidine hydrochlorides and methylarenes: TBHP-mediated synthesis of substituted 1,3,5-triazines under metal-free conditions

机译：idine盐酸盐和甲基芳烃的直接氧化偶联：TBHP介导的无金属条件下合成1,3,5-三嗪

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摘要

Various 2,4,6-trisubstituted 1,3,5-triazines were smoothly formed via TBHP-mediated direct oxidative coupling of amidine and methylarenes. This tandem oxidation-imination-cyclization transformation exhibits a straightforward protocol to prepare 1,3,5-triazines from easily available starting materials and green oxidants under metal-free conditions.

机译：各种2,4,6-三取代的1,3,5-三嗪通过TBHP介导的and和甲基芳烃的直接氧化偶联而顺利形成。此串联氧化-胺化-环化转化过程展示了一种简单的方案，可以在无金属的条件下从容易获得的原料和绿色氧化剂制备1,3,5-三嗪。

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《Organic & biomolecular chemistry 》 |2015年第41期| 10285-10289| 共5页
作者
Wei Guo;
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School of Chemistry & Chemical Engineering, South China University of Technology, Guangzhou 510641, People's Republic of China,Key Laboratory of Organo-Pharmaceutical Chemistry of Jiangxi Province, Gannan Normal University, Ganzhou, 341000, China;

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1. TBHP-mediated oxidative synthesis of substituted pyrimido[4,5-d]pyrimidines from N-uracil amidines and methylarenes under metal free conditions [J] . RSC Advances . 2019 ,第51期

机译：来自N-尿嘧啶脒的取代嘧啶的氧化合成的氧化合成，无金属条件下的N-尿嘧啶和甲基溴
2. TBHP-mediated oxidative synthesis of substituted pyrimido[4,5-d]pyrimidines from N-uracil amidines and methylarenes under metal free conditions [J] . Pradip Debnath RSC Advances . 2019 ,第51期

机译：TBHP介导在无金属条件下由N-尿嘧啶am和甲基芳烃氧化合成取代的嘧啶并[4,5-d]嘧啶
3. Polythene glycol (PEG) as a reusable solvent system for the synthesis of 1,3,5-triazines via aerobic oxidative tandem cyclization of benzylamines and N-substituted benzylamines with amidines under transition metal-free conditions [J] . Tiwari Abhishek R., Bhanage Bhalchandra M. Green chemistry . 2016 ,第1期

机译：聚乙二醇（PEG）作为可重用的溶剂体系，用于在无过渡金属的条件下通过苄胺和N-取代的苄胺与am的需氧氧化串联环化反应来合成1,3,5-三嗪
4. Synthesis of potassium salts of 2,4-diamino(alkylamino)-6-dinitromethyl-1,3,5-triazine and 2-hydrazinyl-4-amino(alkylamino)-6-dinitromethyl-1,3,5-triazine [C] . Alexander A. Gidaspov, Vladimir V. Bakharev, Olga V. Golovina, Seminar on New Trends in Research of Energetic Materials . 2014

机译：2,4-二氨基（烷基氨基）-6-二硝基甲基-1,3,5-三嗪和2-肼基-4-氨基（烷基氨基）-6-二硝基甲基-1,3,5-三嗪的钾盐的合成
5. Biotic and abiotic transformations of hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) mediated by Geobacter metallireducens (GS-15) and iron oxides. [D] . Gregory, Kelvin Bolton. 2002

机译：由金属还原杆菌（GS-15）和氧化铁介导的六氢-1,3,5-三硝基-1,3,5-三嗪（RDX）的生物和非生物转化。
6. TBHP-mediated highly efficient dehydrogenative cross-oxidative coupling of methylarenes with acetanilides [O] . Cui Chen, Weibing Liu, Peng Zhou 2016

机译：TBHP介导的甲基芳烃与乙酰苯胺的高效脱氢交叉氧化偶联
7. TBHP-mediated oxidative synthesis of substituted pyrimido4,5-dpyrimidines fromN-uracil amidines and methylarenes under metal free conditions [O] . Pradip Debnath 2019

机译：TBP介导的嘧米胺的氧化合成4,5-D嘧啶Fromn-Uracil脒和甲基溴如金属条件下
8. Synthesis of 14C-Labelled Octahydor-1,3, 5,7-Tetranitro-1,3,5,7- Tetrazocine HMx0 and 15N-Isotopic Hexahyrro-1,3,5- Trinitro-1,3,5-Triazine (RDX) for use in Microcosm Experiments [R] . Ampleman, G. , Marois, A. , Thiboutot, S. , 2000

机译：14C-标记的Octahydor-1,3,5,7-四硝基-1,3,5,7-四氮杂辛Hmx0和15N-同位素六氢-1,3,5-三硝基-1,3,5-三嗪（RDX）的合成）用于微观世界实验

Direct oxidative coupling of amidine hydrochlorides and methylarenes: TBHP-mediated synthesis of substituted 1,3,5-triazines under metal-free conditions

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