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Characterization of Artificially Shocked forsterites: (1) Diffraction Profile Analysis by Gandolfi Camera

机译:人工冲击的镁橄榄石的表征:(1)Gandolfi相机的衍射轮廓分析

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We have examined synthetic single crystals of forsterites shocked up to 82GPa using a single stage propellant gun. Even in forsterites shocked to 82GPa, any decomposition phases such as spinels or silica glasses and fine-grained MgO could not be detected by X-ray diffraction and EPMA methods. Profile analysis of X-ray diffraction peaks of the shocked forsterites using a Gandolfi camera has been done to detect the maximum strain. The maximum strain derived from Williamson-Hall plot of about 20 diffraction angles and their integral maximum breadths had a linear relation to the shock pressures, in which the elastic limit could not be detected. Unit cell dimensions did not show any changes against the shock pressures, however the increasing broadening of X-ray diffraction peaks occurred with the increase of shock pressures, indicating the homogeneous lattice distortion due to shock pressures. This is the first quantitative analysis that enables us to estimate an experienced shock pressure from the X-ray peak broadening, and is applied to the Dhurmsala LL6 chondrite; the pressure estimated in this study is ranging from 24.0 to 37.8GPa in contrast to the range of 5 to 20 GPa (shock stage S3 by Stoeffler et al, 1991) estimated from the texture of olivine in the chondrite.
机译:我们已经研究了使用单级推进剂枪震荡到82GPa的镁橄榄石的合成单晶。即使在冲击到82GPa的镁橄榄石中,也无法通过X射线衍射和EPMA方法检测到任何分解相,例如尖晶石或石英玻璃和细粒MgO。已经使用Gandolfi相机对震荡的镁橄榄石的X射线衍射峰进行了轮廓分析,以检测最大应变。由Williamson-Hall曲线得出的最大应变约为20个衍射角,其最大积分宽度与冲击压力呈线性关系,其中无法检测到弹性极限。晶胞尺寸没有显示出对冲击压力的任何变化,但是,X射线衍射峰的增宽随着冲击压力的增加而发生,表明由于冲击压力导致的均匀晶格畸变。这是第一个定量分析,它使我们能够从X射线峰展宽来估计经历的冲击压力,并将其应用于Dhurmsala LL6球粒陨石。这项研究估计的压力范围为24.0至37.8GPa,而根据球粒陨石中橄榄石的质地估计的压力范围为5至20 GPa(Stoeffler等,1991年为休克期S3)。

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