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The Effect Of Annealing Temperature On Micro-structure And Mechanical Properties Of C/sic Composites

机译:退火温度对C / SiC复合材料显微组织和力学性能的影响

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In this paper, the rare-earth-oxide La_2O_3 combined with Al_2O_3 served as sintering additives and low-cost α-SiC powder were exploited successfully to prepare dense short carbon fiber reinforced SiC composites by hot-pressing (HP) sintering. The results of the experiments proved that the combination of Al_2O_3 and La_2O_3 sintering additives system was effective to promote densification of the hot-pressed C_f/SiC composites. The influence of the annealed temperature on the micro-structure and mechanical properties of the C_f/SiC composites was investigated in details. The proper annealed condition is favorable to improve the room temperature mechanical properties. The most interesting phenomenon was observed that silicon carbide nano-whisker structure was formed in the material which was annealed at 1750 ℃ for 1 h. It is undoubted that nano-whisker structure would promote fracture toughness. The combination of grain bridging, crack deflection and nano-fiber debonding can improve fracture toughness.
机译:以稀土氧化物La_2O_3和Al_2O_3为烧结助剂,采用低成本的α-SiC粉体,通过热压(HP)烧结成功制备了致密的短碳纤维增强SiC复合材料。实验结果证明,Al_2O_3和La_2O_3烧结助剂体系的组合可有效促进热压C_f / SiC复合材料的致密化。详细研究了退火温度对C_f / SiC复合材料组织和力学性能的影响。适当的退火条件有利于改善室温机械性能。观察到最有趣的现象是在1750℃下退火1 h的材料中形成了碳化硅纳米晶须结构。毫无疑问,纳米晶须结构将促进断裂韧性。晶粒桥接,裂纹变形和纳米纤维剥离的结合可以提高断裂韧性。

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