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Mechanical and Structural Property Changes of Monolithic SiC and Advanced SiC/SiC Composites due to Low Temperature He~+-Ion Irradiation and Post-Irradiation High Temperature Annealing

机译:低温He〜+离子辐照和辐照后高温退火导致整体SiC和高级SiC / SiC复合材料的力学和结构性能变化

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The hardness and elastic modulus of monolithic β-SiC and advanced SiC/SiC composites irradiated to He-concentrations of from 1000 to 20 000 at.ppm at a temperature below 100°C were investigated. Changes in the hardness and elastic modulus were correlated with He release behavior and with irradiation-induced microstructural changes and swelling. The hardness and elastic modulus of the irradiated specimens decreased with He concentration. Amorphized regions were observed in the He-irradiated monolithic β-SiC. The mechanical property changes likely were due to irradiation-induced amorphization. By the annealing at 1200°C, nearly full recovery was achieved. He release peaks from the pyrolitic graphite, monolithic SiC, and the SiC/SiC composites at 250, 700, 1000, and 1150°C, were identified. The correlation between the mechanical property and microstructural changes and the He release behavior are discussed.
机译:研究了在低于100°C的温度下以1000到20000 at.ppm的He浓度辐照的整体式β-SiC和高级SiC / SiC复合材料的硬度和弹性模量。硬度和弹性模量的变化与He释放行为以及辐照引起的微观结构变化和溶胀相关。辐照后样品的硬度和弹性模量随He浓度的降低而降低。在He照射的整体式β-SiC中观察到非晶化区域。机械性能的变化可能是由于辐照引起的非晶化。通过在1200℃下退火,几乎可以完全恢复。他确定了在250、700、1000和1150°C下从热解石墨,单块SiC和SiC / SiC复合材料释放的峰。讨论了力学性能与微观结构变化以及He释放行为之间的相关性。

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