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Experimental investigation on mechanical properties of a fiber-reinforced silica aerogel composite

机译:纤维增强二氧化硅气凝胶复合材料力学性能的实验研究

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Aerogel has been used for thermal insulation because of its extremely low thermal conductivity, but the application has been restricted to non-loading-bearing structures by its low strength properties. Fiber-reinforced aerogel was prepared with higher strength but without sacrificing much of its thermal conductivity. While fiber-reinforced aerogel performs as load-bearing insulation, two behaviors must be investigated: compression and stress relaxation at evaluated temperature. At first, compression test was performed on a fiber-reinforced aerogel composite at both room and evaluated temperature, then the effects of temperature on compression properties of the fiber-reinforced aerogel were analyzed. Stress Relaxation Test was carried out at a constant strain of 0.1 for 1200 s at both room and evaluated temperature. The experimental results show that the stress relaxations increase with the temperature rise from 200℃ to 800℃ Previous research and Scanning Electron Microscope (SEM) analysis of specimens showed that two time-dependent behaviors: (1) cracks induced by collapse of the pores, and (2) fiber failures subject to interfaces that debond and slide, might be possible reasons for the stress relaxation and the small inelastic strain of specimen tested at 25 ℃. While three time dependent phenomena: (1) fusing of aerogel nanoparticles to form nanoparticle clusters, (2) fiber stress relaxation and (3) fiber failures subject to interfaces that debond and slide, would be possible reasons for the remarkable stress relaxation behavior at 800 ℃.
机译:气凝胶由于其极低的热导率而被用于绝热,但由于其低强度特性,其应用已被限制在非承重结构中。纤维增强气凝胶的制备具有较高的强度,但并未牺牲其大部分的热导率。尽管纤维增强的气凝胶起到承重绝缘的作用,但必须研究两种行为:在评估温度下的压缩和应力松弛。首先,在室温和评估温度下对纤维增强气凝胶复合材料进行压缩试验,然后分析温度对纤维增强气凝胶压缩性能的影响。在室温和评估温度下,均以0.1的恒定应变进行应力松弛测试1200 s。实验结果表明,应力松弛随温度从200℃升高到800℃而增加。先前的研究和扫描电子显微镜(SEM)分析的样品显示出两种随时间变化的行为:(1)孔塌陷引起的裂纹; (2)受到界面剥离和滑动影响的纤维失效,可能是应力松弛和在25℃下测试的试样的较小非弹性应变的可能原因。尽管存在三种与时间有关的现象:(1)气凝胶纳米颗粒融合形成纳米颗粒簇;(2)纤维应力松弛;(3)受到界面剥离和滑动的纤维破坏,这可能是800℃时应力松弛行为显着的可能原因。 ℃。

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