首页> 外文期刊>Journal of University of Science and Technology Beijing >Fabrication and characterization of highly ordered Ni_(0.5)Zn_(0.5)Fe_2O_4 nanowire/tube arrays by sol-gel template method
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Fabrication and characterization of highly ordered Ni_(0.5)Zn_(0.5)Fe_2O_4 nanowire/tube arrays by sol-gel template method

机译:溶胶-凝胶模板法制备高序Ni_(0.5)Zn_(0.5)Fe_2O_4纳米线/管阵列及其表征

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摘要

Highly ordered nanowire/tube arrays of Ni_(0.5)Zn_(0.5)Fe_2O_4 were fabricated by the sol-gel method in the pores of anodic alumina membrane (AAM). Whether nanowires or nanotubes were fabricated depends on immersion time. The immersion time was 15-40 s for nanotubes and over 60 s for nanowires. The topography and crystalline structure of the nanowire arrays were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), and X-ray diffraction (XRD). It was found that the length and diameter of the Ni_(0.5)Zn_(0.5)Fe_2O_4 nanowires are related to the thickness of the AAM and the diameter of the pores. The results indicated that the Ni_(0.5)Zn_(0.5)Fe_2O_4 nanowires are uniform and parallel to each other.
机译:通过溶胶-凝胶法在阳极氧化铝膜(AAM)的孔中制备了Ni_(0.5)Zn_(0.5)Fe_2O_4的高序纳米线/管阵列。纳米线或纳米管的制造取决于浸入时间。纳米管的浸入时间为15-40 s,纳米线的浸入时间为60 s以上。纳米线阵列的形貌和晶体结构通过扫描电子显微镜(SEM),透射电子显微镜(TEM)和X射线衍射(XRD)表征。发现Ni_(0.5)Zn_(0.5)Fe_2O_4纳米线的长度和直径与AAM的厚度和孔的直径有关。结果表明,Ni_(0.5)Zn_(0.5)Fe_2O_4纳米线均匀且相互平行。

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