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Auto-combustion preparation and characterization of lead titanate nanoparticles by using different acids and its photocatalyst application

机译:不同酸在钛酸铅纳米粒子上的自动燃烧制备与表征及其光催化剂的应用

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摘要

The effect of different acids such as cinnamic acid, salicylic acid, and oxalic acid on size, morphology and uniformity of PbTiO_3 nanoparticles prepared via a auto-combustion sol-gel route was investigated. The structural, morphological, and optical properties of as-obtained products were characterized by techniques such as electron dispersive X-ray spectroscopy, X-ray diffraction, scanning electron microscopy and ultraviolet-visible spectroscopy. The estimated band gap shows that this product may be used as a photocatalyst, so the photocatalytic test was performed by photooxidation of methyl orange under UV irradiation and in the presence of PbTiO_3. The results showed that methyl orange degradation was about 95% under for 50 min, so the synthesized product can be used as an effective photocatalyst. Vibrating sample magnetometer was used to study the magnetism properties of PbTiO_3 sample.
机译:研究了肉桂酸,水杨酸和草酸等不同酸对通过自动燃烧溶胶-凝胶法制备的PbTiO_3纳米粒子的尺寸,形貌和均匀性的影响。所获得的产物的结构,形态和光学性质通过电子分散X射线光谱,X射线衍射,扫描电子显微镜和紫外可见光谱等技术表征。估计的带隙表明该产物可以用作光催化剂,因此通过甲基橙在紫外线照射下和PbTiO_3存在下的光氧化反应进行光催化测试。结果表明,在50min下,甲基橙的降解率约为95%,因此该合成产物可作为有效的光催化剂。用振动样品磁力计研究了PbTiO_3样品的磁性。

著录项

  • 来源
    《Journal of materials science》 |2017年第8期|6125-6130|共6页
  • 作者

    S. A. Hoseini;

  • 作者单位

    Young Researchers and Elite Club, South Tehran Branch, Islamic Azad University, Tehran, Iran;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

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