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Structural studies on the yttrium-doped cobalt ferrite powders synthesized by sol-gel combustion method

机译:溶胶凝胶燃烧法合成钇掺杂钴铁氧体粉末的结构研究

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摘要

Y_(0.2)CoFe_(1.8)O_4 nanopowders were prepared using a sol-gel combustion method. Metal nitrates, such as yttrium nitrate, cobalt nitrate and ferric nitrate, were used as the source materials. Citric acid and polyvinyl alcohol were used as the burning agent and agglomeration reducing agent, respectively. The pH of the precursor was maintained at 7. The mean crystallite size of the prepared ferrite was in the range of ~20-70nm. The inverse spinel structure, cubic morphology, and the identification of functional groups of the yttrium-doped cobalt ferrite were analyzed systematically using several analytical tools.
机译:使用溶胶-凝胶燃烧法制备了Y_(0.2)CoFe_(1.8)O_4纳米粉。金属硝酸盐(例如硝酸钇,硝酸钴和硝酸铁)用作原料。柠檬酸和聚乙烯醇分别用作燃烧剂和结块减少剂。前驱体的pH值保持在7。制得的铁氧体的平均晶粒尺寸在〜20-70nm的范围内。使用几种分析工具系统地分析了尖晶石的反向结构,立方形貌以及掺杂钇的钴铁氧体的官能团的鉴定。

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  • 来源
    《Journal of magnetism and magnetic materials》 |2012年第14期|p.2245-2248|共4页
  • 作者单位

    Center for Advanced Material Technology, Kookmin University, 861-1 Jeongneung-dong Seongbuk-gu, Seoul 136-702, Republic of Korea;

    School of Advanced Materials Engineering, Kookmin University, jeongneung-dong, Seongbuk-gu, Seoul 136-702, Republic of Korea;

    School of Advanced Materials Engineering, Kookmin University, jeongneung-dong, Seongbuk-gu, Seoul 136-702, Republic of Korea;

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  • 原文格式 PDF
  • 正文语种 eng
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  • 关键词

    sol-gel; nanocrystallite; structural characterization; morphology;

    机译:溶胶凝胶纳米微晶结构表征;形态学;

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