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Magnetic Properties of FeCo Films Prepared by Co-Sputtering and Hydrogenous Gas Reactive Sputtering

机译:共溅射和氢气反应溅射制备的FeCo薄膜的磁性

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In this experiment, we have added carbon into FeCo films by two kinds of sputtering processes: the first is the conventional process of co-sputtering, the second is introducing hydrogenous gas (acetylene gas in this experiment) into the chamber during sputtering. The crystallographic, microstructure, and magnetic properties of the films have been compared. Although nano-crystalline films, which have much lower coercivity according to the random anisotropy theory proposed by Herzer in 1990, can be prepared by both processes, magnetic properties of the films prepared by the two processes are different. Magnetic soft films are successfully prepared with coercivity about 1 Oe, saturation magnetization about 23.5 kG, and real part permeability as large as 1200–1500 in the frequency range up to 2.6 GHz. X-ray photoelectron spectroscopy results show films deposited without hydrogenous gas have oxygen contamination as high as 3 at%. Oxygen-free films are found to be prepared with the introducing of acetylene gas during the sputtering process.
机译:在本实验中,我们通过两种溅射工艺将碳添加到了FeCo膜中:第一种是常规的共溅射工艺,第二种是在溅射过程中将氢气(本实验中的乙炔气)引入腔室。比较了薄膜的晶体学,微观结构和磁性。尽管可以通过两种方法制备根据Herzer在1990年提出的随机各向异性理论具有低得多的矫顽力的纳米晶体膜,但是通过两种方法制备的膜的磁性能不同。磁性软膜已成功制备,矫顽力约为1 Oe,饱和磁化强度约为23.5 kG,在高达2.6 GHz的频率范围内,实部磁导率高达1200-1500。 X射线光电子能谱结果表明,在没有氢气的情况下沉积的膜的氧污染高达3at%。发现在溅射过程中通过引入乙炔气体来制备无氧薄膜。

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