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Characterization of Chemically Activated Carbons Produced from Coconut and Palm Kernel Shells Using SEM and FTIR Analyses

机译:利用SEM和FTIR分析表征从椰子和棕榈核壳中产生的化学活性碳的特征

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Chemically activated carbons generated from coconut (CS) and palm kernel (PKS) shells soaked with 1M solution of K_(2)CO_(3) and NaHCO_(3) at 1000°C using the Carbolite Muffle Furnace were examined using scanning electron microscopy (SEM) and Fourier Transformation Infrared Spectroscopy (FTIR). Results from the FTIR analyses revealed that the coconut and palm kernel shells manufactured were successfully chemically activated. Several chemical compounds and functional groups, such as hydroxyl groups, carbonyl groups, ethers, alkanes, alkenes, and aromatic groups, were detected in chemically activated carbon produced from palm kernels and coconut shells as proof of the lignocellulose structure in them. Chemically activated carbon made from coconut shells exhibited nine distinct spectra, while palm kernel shells exhibited six distinct spectra. The pores were larger in the chemically activated carbons produced at a higher temperature (1000°C), demonstrating that temperature is an essential process parameter in the development of surface porosity in chemically activated carbons. The chemical carbonization activation methods used provided porosity, a large surface area, and precise morphology for absorption in both the coconut and palm kernel shells, indicating that they can be turned to high-performance adsorbents. Both organic and inorganic contaminants can be removed from the environment using the chemically activated carbons produced.
机译:使用扫描电子显微镜检查从100M溶液浸入100M溶液的椰子(CS)和棕榈核(PKS)壳浸没在1000℃的k_(2)CO_(3)和NaHCO_(3)的壳中的壳( SEM)和傅里叶变换红外光谱(FTIR)。 FTIR分析的结果表明,制造的椰子和棕榈仁壳成功化学活化。在由棕榈仁和椰子壳生产的化学活性炭中检测到几种化学化合物和官能团,例如羟基,羰基,醚,烷烃,烯烃和芳族基团作为木质纤维素结构的证据。由椰子壳制成的化学活性炭表现出九个不同的光谱,而棕榈核壳均显示出六种不同的光谱。在更高温度(1000℃)的化学活性炭中孔隙较大,证明温度是化学活化碳中表面孔隙率的基本过程参数。化学碳化活化方法使用孔隙率,大表面积和精确的形态,用于椰子和棕榈核壳中的吸收,表明它们可以转向高性能的吸附剂。可以使用产生的化学活性碳,从环境中除去有机和无机污染物。

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