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Optimisation of mechanical stir casting parameters for fabrication of carbon nanotubes–aluminium alloy composite through Taguchi method

机译:Taguchi法优化制备碳纳米管-铝合金复合材料的机械搅拌铸造参数

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The liquid metallurgical process route for synthesis of multiwalled carbon nanotube–A356 aluminium alloy (MWCNT-A356) composite is suitable for intricate designs and bulk production. In this work, MWCNT-CNT was fabricated through mechanical stir casting followed by thixoforming and modified by T6 (MT6) heat treatment. Hence, the optimisation and effect of variables such as amount of CNT, amount of wettability agent of Mg and mechanical stirring duration were investigated using a robust design of experiment (DOE), namely, Taguchi method, with two factorial levels. The signal-to-noise (S/N) ratio (‘larger is better’), hardness and ultimate tensile strength (UTS) were used as response variables. Results showed that the optimum hardness and UTS values of 106.4HV and 277.0MPa, respectively, were obtained from the nanoncomposite subjected to DOE run 4 and containing 0.5wt.% MWCNT, 0.5wt.% Mg and 10min of mechanical stirring. The hardness (76.3%) and UTS (108.4%) improved compared with those of the as-cast A356 alloy. The transformation of the microstructures and the porosity of the as-cast after thixoforming and MT6 modification were also discussed. This work demonstrated the optimised mechanical stir casting parameters for MWCNT-A356 fabrication and the enhanced mechanical properties achieved by thixoforming and heat treatment.
机译:用于合成多壁碳纳米管– A356铝合金(MWCNT-A356)复合材料的液态冶金工艺路线适合复杂的设计和批量生产。在这项工作中,通过机械搅拌铸造,触变成型并通过T6(MT6)热处理对MWCNT-CNT进行制造。因此,使用稳健的实验设计(DOE),即Taguchi方法,以两个因子水平研究了CNT量,Mg润湿剂的量和机械搅拌持续时间等变量的优化和效果。信噪比(S / N)(“越大越好”),硬度和极限抗拉强度(UTS)被用作响应变量。结果表明,由经过DOE运行4且含有0.5wt。%MWCNT,0.5wt。%Mg和10分钟机械搅拌的纳米复合材料获得的最佳硬度和UTS值分别为106.4HV和277.0MPa。与铸造的A356合金相比,硬度(76.3%)和UTS(108.4%)提高了。还讨论了触变成型和MT6改性后的铸态组织和孔隙率。这项工作证明了用于MWCNT-A356制造的最佳机械搅拌铸造参数以及通过触变性和热处理获得的增强的机械性能。

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