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首页> 外文期刊>X-ray Structure Analysis Online >Synthesis and Structure of 3,3′-[(4-Benzyloxyphenyl)methylene]bis-(4-hydroxy-2H-chromen-2-one)
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Synthesis and Structure of 3,3′-[(4-Benzyloxyphenyl)methylene]bis-(4-hydroxy-2H-chromen-2-one)

机译:3,3'-[(4-苄氧基苯基)亚甲基]双-(4-羟基-2H-铬-2--2-)的合成与结构

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The structure of 3,3′-[(4-benzyloxyphenyl)methylene]bis-(4-hydroxy-2H-chromen-2-one) was determined by X-ray crystallography The compound crystallized in a monoclinic system and was characterized thus: P21/n, a = 12.2990(15)Å, b = 10.8108(8)Å, c = 21.277(2)Å, Z = 4, V = 2787.7(5)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0860 and R2 = 0.1436.
机译:通过X-射线晶体学测定3,3′-[((4-苄氧基苯基)亚甲基]双-(4-羟基-2H-铬烯-2-酮)的结构。单斜系统,其特征是: P 2 1 / n , a = 12.2990(15)Å, b = 10.8108(8)Å, c = 21.277(2)Å, Z = 4, V = 2787.7(5)Å 3 。通过直接方法解析晶体结构,并通过 F 2 上的全矩阵最小二乘法将其精炼为最终值 R 1 = 0.0860和 R 2 = 0.1436。

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