首页> 外文期刊>Química Nova >Aplica??o de métodos quimiométricos na caracteriza??o de charutos utilizando extra??o por dispers?o da matriz em fase sólida e análise por cromatografia gasosa acoplada à espectrometria de massas
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Aplica??o de métodos quimiométricos na caracteriza??o de charutos utilizando extra??o por dispers?o da matriz em fase sólida e análise por cromatografia gasosa acoplada à espectrometria de massas

机译:化学计量学方法在通过固相基质分散萃取和气相色谱-质谱联用分析法在雪茄表征中的应用

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In this work, the organic compounds of cigar samples from different brands were analyzed. The compound extraction was made using the matrix solid-phase dispersion (MSPD) technique, followed by gas chromatography and identification by mass spectrometry (GC-MS) and standards, when available. Thirty eight organic compounds were found in seven different brands. Finally, with the objective of characterizing and discriminating the cigar samples, multivariate statistical analyses were applied to data, e.g.; principal component analysis (PCA) and hierarchical cluster analysis (HCA). With such analyses, it was possible to discriminate three main groups of three quality levels.
机译:在这项工作中,分析了来自不同品牌的雪茄样品的有机化合物。使用基质固相分散体(MSPD)技术提取化合物,然后进行气相色谱分析,并通过质谱(GC-MS)和标准品(如果有)进行鉴定。在七个不同的品牌中发现了38种有机化合物。最后,为了表征和区分雪茄样品,对数据进行多变量统计分析,例如主成分分析(PCA)和层次聚类分析(HCA)。通过这样的分析,可以区分三个质量等级的三个主要组。

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