An Efficient and Green Method for Synthesis of 2,4,5-Triarylimidazoles without Use of Any Solvent, Catalyst, or Solid Surface

SwatiSamanta; SaheliSarkar; RammohanPal; Asok K.Mallik

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An Efficient and Green Method for Synthesis of 2,4,5-Triarylimidazoles without Use of Any Solvent, Catalyst, or Solid Surface

机译：无需使用任何溶剂，催化剂或固体表面即可合成2,4,5-三芳基咪唑的高效绿色方法

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An efficient and green method for synthesis of 2,4,5-triarylimidazoles without use of any catalyst or solvent has been developed simply by heating (at 130°C) of mixtures of 1,2-diketone, aromatic aldehyde, and ammonium acetate in 1 : 1 : 3 mole ratio.

机译：通过简单地（在130°C下）加热1,2-二酮，芳族醛和乙酸铵的混合物（在130°C下），已开发出一种无需使用任何催化剂或溶剂即可合成2,4,5-三芳基咪唑的高效绿色方法。 1：1：3摩尔比。

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《Organic Chemistry International》 |2013年第1期|共5页
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SwatiSamanta; SaheliSarkar; RammohanPal; Asok K.Mallik;
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1. A simple and straightforward method for one-pot synthesis of 2,4,5- triarylimidazoles using titanium dioxide as an eco-friendly and recyclable catalyst under solvent-free conditions [J] . Goutam Brahmachari, Suvankar Das Indian Journal of Chemistry, Section B. Organic Including Medicinal . 2013,第3期

机译：一种简单直接的方法，可在无溶剂条件下使用二氧化钛作为环保和可回收的催化剂，一锅合成2,4,5-三芳基咪唑
2. Facile Method for One-Step Synthesis of 2,4,5-Triarylimidazoles Under Catalyst-Free, Solvent-Free, and Microwave-Irradiation Conditions [J] . Synthetic Communications . 2010,第8期

机译：在无催化剂，无溶剂和微波辐射条件下一步合成2,4,5-三芳基咪唑的简便方法
3. Facile method for one-step synthesis of 2,4,5-triarylimidazoles under catalyst-free, solvent-free, and microwave-irradiation conditions [J] . Zhou J.-F., Gong G.-X., Sun X.-J., Synthetic Communications . 2010,第7a9期

机译：在无催化剂，无溶剂和微波辐射条件下一步合成2,4,5-三芳基咪唑的简便方法
4. Coaled carbon-based solid acid: A new and efficient catalyst for click synthesis of 3,4-dihydropyrimidin-2(1H)-ones under solvent-free conditions [C] . Liu Wanyi, Ning Liu, Ruiyuan Zheng, International Conference on Chemical, Material and Metallurgical Engineering . 2013

机译：含有碳化碳固体酸：在无溶剂条件下单击合成3,4-二氢嘧啶-2（1H）酮的新增有效的催化剂
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. An Efficient Protocol for the Green and Solvent-Free Synthesis of Azine Derivatives at Room Temperature Using BiCl3-Loaded Montmorillonite K10 as a New Recyclable Heterogeneous Catalyst [O] . K. Ravi, B. Krishnakumar, M. Swaminathan 2012

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机译：甘油作为绿色溶剂，用于高效，一锅法和无催化剂合成2,4,5-三芳基和1,2,4,5-四芳基咪唑衍生物

An Efficient and Green Method for Synthesis of 2,4,5-Triarylimidazoles without Use of Any Solvent, Catalyst, or Solid Surface

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