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Facile Preparation of Hydrophobic Aluminum Oxide Film via Sol-Gel Method

机译:溶胶-凝胶法快速制备疏水性氧化铝膜

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Hydrophobic aluminum oxide films (AOFs) are widely used in anti-oxidation and anti-corrosion applications. In preparing AOFs, complex and high temperature conditions are usually necessary. Here, we report aluminum nanowire structures with hydrophobic properties, prepared using a facile sol-gel method by magnetic stirrer and hydrothermal reaction. The electromagnetic force work has great influence on the structure of AOFs. The surface morphology and compositions of the AOFs were analyzed by scanning electron microscope (SEM), energy dispersive X-ray spec-trometers (EDS), X-ray diffraction (XRD), 3M peeling test and X-ray photoelectron spectroscopy (XPS). With the increase of water content in hydrothermal reaction, the hydrophobicity of AOFs proportional increased. Adding 10 ml deionized water leads to the formation of the upper nanowires and the lower nanohole with 129.3 ° water contact angle. Meanwhile, the AOF provide a good substrate for electroless deposition (ELD) of copper (Cu) to achieve a simple fabrication of metal conductor.
机译:疏水氧化铝膜(AOF)广泛用于抗氧化和防腐应用。在制备AOF时,通常需要复杂的高温条件。在这里,我们报告铝纳米线结构具有疏水性,通过使用磁力搅拌器和水热反应的溶胶凝胶法制备的。电磁力功对AOF的结构有很大的影响。通过扫描电子显微镜(SEM),能量色散X射线光谱仪(EDS),X射线衍射(XRD),3M剥离试验和X射线光电子能谱(XPS)分析了AOF的表面形态和成分。随着水热反应中水含量的增加,AOFs的疏水性成比例增加。添加10 ml去离子水导致形成上纳米线和下纳米孔,水接触角为129.3°。同时,AOF为铜(Cu)的化学沉积(ELD)提供了良好的衬底,以实现金属导体的简单制造。

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