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THE USE OF GLASS TRANSITION TEMPERATURE IN FORECASTING WHEY POWDER STORAGE STABILITY OBTAINED BY ELECTRO-SPARK TREATMENT

机译:玻璃化转变温度在预测电火花处理获得的乳清粉存储稳定性中的应用

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This study investigated the behavior during storage of dry whey obtained using different approaches that prevent caking (by adding silicon dioxide, electro-spark treatment of whey). Forecasting the stability of quality whey powder was carried out based on a glass transition temperature.The glass transition temperature of whey powder was measured by differential scanning calorimetry.We showed that the highest glass transition temperature (+18.5 °С) and,subsequently, the smallest difference between product temperatures and glass transition temperature were discovered in dry whey, obtained with the use of electro-spark treatment, which proved to be stable during storage.We have found that the other samples of dry whey under normative storing conditions (from 0 till 20 °С) are predominantly in rubbery state, which can influence negatively the stability of the product during storage. Based on the glass transition temperature we determined that electro-spark treatment used in the technology of whey powder allowed reaching anti-caking effect due to physico-chemical processes resulting from electro-spark charges. This was proved by calculating the stickiness and caking sensibility index and the degree of caking (to 2 %). It was experimentally proved that the dry milk whey produced with electro-spark treatment differed positively from other samples by absence of non-fermentative darkening.Whey powder produced from whey treated with electro-spark charges was characterized by the highest degree of whiteness, which did not significantly change in 8 month storage.
机译:这项研究调查了干乳清粉在储存过程中的行为,这些干乳粉使用不同的方法来防止结块(通过添加二氧化硅,电火花处理乳清)。根据玻璃化转变温度预测优质乳清粉的稳定性,通过差示扫描量热法测量乳清粉的玻璃化转变温度,结果显示最高玻璃化转变温度(+18.5°С),其后为在使用电火花处理得到的干乳清中发现产品温度和玻璃化转变温度之间的最小差异,在存储过程中被证明是稳定的。我们发现其他干乳清样品在标准存储条件下(从0开始直到20°С)主要处于橡胶态,这会对产品在储存过程中的稳定性产生负面影响。根据玻璃化转变温度,我们确定,由于电火花电荷产生的物理化学过程,乳清粉技术中使用的电火花处理可以达到抗结块效果。通过计算粘性和结块敏感性指数以及结块程度(至2%)来证明这一点。实验证明,经电火花处理的乳清粉与其他样品的区别在于无发酵变黑。乳清粉经电火花处理后产生的乳清粉具有最高的白度特征。 8个月的存储空间没有明显变化。

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