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Preparation, Characterization and Stabilization of Nano-sized Copper Particles

机译:纳米铜粒子的制备,表征和稳定性

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Cu nanoparticles dispersed in water were prepared by the reduction of Cu+2 originated from the copper salt solution. The stability of the Cu nanoparticles in dispersion was monitored through the analysis of the absorbance spectra at different stages during the process of synthesis. The stability of the Cu nanoparticles dispersed in aqueous medium was investigated after different time intervals. Cu colloid was found to be stable up to 18 hours without major aggregation under atmospheric condition. The size and size distribution of the particles were examined by particle size analyzer. The morphology of the particle synthesised was examined by SEM and AFM. After 24 hours of storage in open air there was some agglomeration of nanoparticles as observed by particle size analyzer and AFM studies. But found stable with the use of 1 % trisodium citrate as stabilizer.
机译:通过还原源自铜盐溶液的Cu + 2,可以制备分散在水中的Cu纳米粒子。通过分析合成过程中不同阶段的吸收光谱,可以监测铜纳米颗粒在分散液中的稳定性。在不同的时间间隔后,研究了分散在水性介质中的铜纳米粒子的稳定性。发现铜胶体在大气条件下长达18小时稳定,且没有主要聚集。通过粒度分析仪检查颗粒的尺寸和尺寸分布。通过SEM和AFM检查合成的颗粒的形态。在露天储存24小时后,通过粒度分析仪和AFM研究观察到纳米颗粒发生了一些团聚。但发现使用1%柠檬酸三钠作为稳定剂是稳定的。

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