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Evaluation of Thermal and Physical Properties of Magnesium Nitride Powder: Impact of Biofield Energy Treatment

机译:氮化镁粉的热和物理性质评估:生物场能量处理的影响

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Magnesium nitride (Mg3N2) has gained extensive attention due to its catalytic and optoelectronic properties. The present investigation was aimed to evaluate the effect of biofield energy treatment on physical and thermal properties of Mg3N2 powder. The Mg3N2 powder was divided into two parts i.e. control and treated. The control part was remained as untreated and the treated part was subjected to the Mr. Trivedi’s biofield energy treatment. Subsequently, the control and treated Mg3N2 samples were characterized using differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and X-ray diffraction (XRD). The DSC results showed the specific heat capacity of 2.24 Jg-1°C-1 in control, which increased upto 5.55 Jg-1°C-1 in treated Mg3N2 sample. The TGA data revealed that the onset temperature for the formation of magnesium oxide, possibly due to oxidation of Mg3N2 in the presence of air and moisture, was reduced from 421.0°C (control) to 391.33°C in treated sample. Besides, the XRD data revealed that the lattice parameter and unit cell volume of treated Mg3N2 samples were increased by 0.20 and 0.61% respectively, as compared to the control. The shifting of all peaks toward lower Bragg angle was observed in treated sample as compared to the control. The XRD diffractogram also showed that the relative intensities of all peaks were altered in treated sample as compared to control. In addition, the density of treated Mg3N2 was reduced by 0.60% as compared to control. Furthermore, the crystallite size was significantly increased from 108.05 nm (control) to 144.04 nm in treated sample as compared to the control. Altogether data suggest that biofield energy treatment has substantially altered the physical and thermal properties of Mg3N2 powder. Thus, the biofield treatment could be applied to modulate the catalytic and optoelectronic properties of Mg3N2 for chemical and semiconductor industries.
机译:氮化镁(Mg3N2)由于其催化和光电特性而受到广泛关注。本研究旨在评估生物场能量处理对Mg3N2粉末的物理和热性能的影响。 Mg 3 N 2粉末分为两部分,即对照和处理。对照部分保持未处理状态,处理过的部分接受了特里维迪先生的生物场能量处理。随后,使用差示扫描量热法(DSC),热重分析(TGA)和X射线衍射(XRD)对对照和处理过的Mg3N2样品进行表征。 DSC结果显示,对照中的比热容为2.24 Jg-1°C-1,在处理过的Mg3N2样品中,比热容增加至5.55 Jg-1°C-1。 TGA数据表明,在空气和湿气存在下,可能由于Mg3N2的氧化,形成氧化镁的起始温度从处理后的样品的421.0°C(对照)降至391.33°C。此外,XRD数据显示,与对照相比,处理后的Mg3N2样品的晶格参数和晶胞体积分别增加了0.20%和0.61%。与对照相比,在处理过的样品中观察到所有峰都向较低的布拉格角移动。 XRD衍射图还显示,与对照相比,在处理的样品中所有峰的相对强度都改变了。此外,与对照相比,处理后的Mg3N2的密度降低了0.60%。此外,与对照相比,处理样品中的微晶尺寸从108.05nm(对照)显着增加至144.04nm。总的数据表明,生物场能量处理已大大改变了Mg3N2粉末的物理和热学性质。因此,生物场处理可用于调节Mg3N2在化学和半导体工业中的催化和光电性能。

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