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Hydroxyapatite Coating on Alloys CoCrMo-TiN with Sol-Gel Method

机译:溶胶-凝胶法在钴铬钼钛合金上涂覆羟基磷灰石

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Hydroxyapatite is synthesized by precipitation-sonification using calcium from field snail shell and powder phosphorus from (NH 4 ) 2 HPO 4. The calcium value was measured by atomic absorption spectrophotometer was 82.82%.The temperatures were varied on 600, 800, and 1000 o C to determine the best temperature of the coating. The best temperature was used to superimpose the HAp on the CoCrMo-TiN metal alloy using the modified sol-gel method. The layer on the metal alloy was identified with x-ray diffraction (XRD) and corrosion test. The XRD result showed that most of the CoCrMo-TiN metal alloy surface was coated by HAp. Beside HAp, there were several other phases such as calcium phosphate, carbonate apatite type A and type B. The best result of the corrosion test was showed in CoCrMo-TiN metal alloy coated with HAp with the smallest corrosion rate 0.0082 mpy.
机译:羟基磷灰石是利用田螺壳中的钙和(NH 4)2 HPO 4中的磷粉通过沉淀声化法合成的。原子吸收分光光度计测得的钙值为82.82%。温度分别在600、800和1000 o C确定涂层的最佳温度。使用改进的溶胶-凝胶法,使用最佳温度将HAp叠加在CoCrMo-TiN金属合金上。通过X射线衍射(XRD)和腐蚀测试来鉴定金属合金上的层。 XRD结果表明,大多数CoCrMo-TiN金属合金表面均被HAp覆盖。除HAp之外,还有其他几个相,例如磷酸钙,碳酸盐磷灰石A型和B型。腐蚀试验的最佳结果显示在涂有HAp的CoCrMo-TiN金属合金中,腐蚀速率最小,为0.0082 mpy。

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