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Characterization Of The Graded Microstructure In Powder Sintered Porous Titanium

机译:粉末烧结多孔钛合金中梯度组织的表征

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The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300?°C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37?°C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37?°C.
机译:所提出的烧结工艺在烧结的钛粉中产生孔隙率和功能梯度的微观结构。在建议的温度区域在1200和1300?C的温度下烧结不同微米尺寸的钛粉2小时。通过在37℃的Hanks平衡盐溶液中进行浸没试验,观察到在渐变的微结构上形成的磷灰石。钛粉的烧结条件通过热重分析-差热分析(​​TG-DTA)估算。通过场发射扫描电子显微镜(FE-SEM)观察和能量色散X射线光谱(EDS)分析表征了合成的表面结构和磷灰石形成能力。结果,这些梯度烧结的多孔钛粉的微观结构显示了在37℃下的Hanks平衡盐溶液(HBSS)中通过钙化形成骨结合而形成的磷灰石形成能力。

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