CHARACTERIZATION OF THE GRADED MICROSTRUCTURE IN POWDER SINTERED POROUS TITANIUM

摘要

The proposed sintering process produce porosity and functional graded microstructure in the sinterd titanium powders. Titanium powders with different micro sizes were sintered at the proposed temperature region at 1200 and 1300 degrees C for 2h. The apatite-forming on the graded microstructure is observed by immersion test in Hanks balanced salt soluion at 37 degrees C. Sintering condition of titanium powders is estimated by thermogravitmetry-differential thermal analysis (TG-DTA). The synthersied surface structures and apatite-forming ability were characterized by a field emission scanning electron microscopy (FE-SEM) observation and energy dispersive X-ray spectroscopy (EDS) analysis. As results, these graded microstructure of sintered porous titanium powders reveals apatite-forming ability as osseointegration by calcification in Hanks balanced salt soluion(HBSS) at 37 degrees C.