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Correlation between the beam profile from a curing light and the microhardness of four resins

机译:固化光的光束轮廓与四种树脂的显微硬度之间的相关性

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Objective. To demonstrate the effect of localized irradiance and spectral distribution inhomogeneities of one LED-based dental light-curing unit (LCU) on the corresponding microhardness values at the top, and bottom surfaces of four dental resin-based composites (RBCs), which contained either camphorquinone (CQ) alone or a combination of CQ and monoacylphosphine oxide (TPO) as photoinitiators. Methods. Localized irradiance beam profiles from a polywave LED-based LCU were recorded five times using a laser beam analyzer, without and with either a 400 nm or 460 nm narrow bandpass filter placed in front of the camera lens. Five specimens of each of the four RBCs (two containing CQ/TPO and two containing CQ-only) were exposed for 5-, 10-, or 30-s with the light guide directly on the top surface of the RBC. After 24 h, Knoop microhardness values were measured at 45 locations across the top and bottom surfaces of each specimen. Microhardness readings for each RBC surface and exposure time were correlated with localized patterns of the LCU beam profile, measured using the 400 nm and 460 nm bandpass filters. Spearman rank correlation was used to avoid relying on an assumption of a bivariate normal distribution for the KHN and irradiance. Results. The local irradiance and spectral emission values were not uniformly distributed across the light tip. There was a strong significant positive correlation with the irradiance beam profile values from the LCU taken through bandpass filters and the microhardness maps of the RBC surfaces exposed for 5 and 10 s. The strength of this correlation decreased with increasing exposure time for the RBCs containing CQ only, and increased for the RBCs containing both CQ and TPO. Conclusions. Localized beam and spectral distributions across the tip end of the light guide strongly correlated with corresponding areas of microhardness in both the top and bottom surfaces among four RBCs with different photoinitiator contents. Significance. A light-curing unit with a highly inhomogeneous light output can adversely affect localized microhardness of resin-based composites and this may be a contributing factor for premature failure of a restoration.
机译:目的。演示一个基于LED的牙科光固化单元(LCU)的局部辐照度和光谱分布不均匀性对四种基于牙科树脂的复合材料(RBC)的顶部和底部表面和底部对应的显微硬度值的影响单独使用樟脑醌(CQ)或将CQ与单酰基氧化膦(TPO)组合用作光引发剂。方法。使用激光束分析仪将基于多波LED的LCU的局部辐照光束轮廓记录了五次,没有在相机镜头前放置400 nm或460 nm窄带通滤光片。将四个RBC中的每一个的五个样本(两个包含CQ / TPO,两个仅包含CQ)暴露5,10或30 s,光导直接位于RBC的上表面。 24小时后,在每个样品的顶面和底面的45个位置测量努氏显微硬度值。每个RBC表面和曝光时间的显微硬度读数与LCU光束轮廓的局部图案相关,该图案使用400 nm和460 nm带通滤光片测量。 Spearman秩相关用于避免依赖KHN和辐照度的二元正态分布的假设。结果。局部辐照度和光谱发射值在整个灯头上分布不均匀。与通过带通滤光片的LCU发出的辐照光束轮廓值和暴露5到10 s的RBC表面的显微硬度图有很强的正相关。这种相关性的强度随着仅包含CQ的RBC的暴露时间的增加而降低,而对于同时包含CQ和TPO的RBC的暴露时间增加。结论。跨越光导尖端的局部光束和光谱分布与四个具有不同光引发剂含量的RBC中上,下表面的相应显微硬度区域密切相关。意义。光输出高度不均匀的光固化单元会不利地影响树脂基复合材料的局部显微硬度,这可能是修复体过早失效的一个重要因素。

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