KAl(SO4)2·12H2O (Alum) Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4(3H)-quinazolinone under Microwave Irradiation and Solvent Free Conditions

Ali A. Mohammadi; S. S. Sadat Hossini

首页> 外文期刊>Chinese Journal of Chemistry >KAl(SO₄)₂·12H₂O (Alum) Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4(3H)-quinazolinone under Microwave Irradiation and Solvent Free Conditions

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KAl(SO₄)₂·12H₂O (Alum) Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4(3H)-quinazolinone under Microwave Irradiation and Solvent Free Conditions

机译：KAl（SO _{4 ）_{2 ·12H _{2 O（明矾）催化2-烷基和2-芳基一锅三组分合成-4（3H）-喹唑啉酮在微波辐射和无溶剂条件下}}}

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Twenty 2,3-disubstituted-4(3H)-quinazolinones were synthesed by one-pot three-component method with isatoic anhydride, orthoesters and amines as raw materials in the presence of KAl(SO₄)₂·12H₂O (Alum) under microwave irradiation and solvent-free conditions. 6-Bromo-2-propyl-3-p-tolylquinazolin-4(3H)-one (4m), 6-bromo-2-methyl-3-phenethylquinazolin-4(3H)-one (4n) and 6-bromo-2-ethyl-3-phenethylquinazolin-4(3H)-one (4o) were characterized by IR, 1H NMR, 13C NMR and elemental analysis.

机译：在KAl（SO _{4 ）<存在的条件下，以等角酸酐，原酸酯和胺为原料，通过一锅三组分法合成了二十种2,3-二取代-4（3H）-喹唑啉酮。 sub> 2 ·12H _{2 O（明矾）在微波辐射和无溶剂条件下进行。 6-溴-2-丙基-3-对甲苯基喹唑啉-4（3H）-一个（4m），6-溴-2-甲基-3-苯乙基喹唑啉-4（3H）-一个（4n）和6-溴-通过IR， 1 NMR， 13 NMR和元素分析对2-乙基-3-苯乙基喹唑啉-4（3H）-一（4o）进行表征。}}

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来源
《Chinese Journal of Chemistry》 |2011年第9期|1982-1984|共3页
作者
Ali A. Mohammadi; S. S. Sadat Hossini;
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作者单位

Department of Chemistry Sabzevar Branch Islamic Azad University Sabzevar Iran;

University of Applied Science and Technology Tehran P. O. Box 14155-1644 Tehran Iran;

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正文语种 eng
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isatoic anhydride; orthoesters; ammonium acetate; 4(3H)-quinazolinone; multi component; microwave-assisted reactions;

机译：异丙酸酐;原酸酯;乙酸铵;4（3H）-喹唑啉酮;多组分;微波辅助反应;

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机译：微波辐射和无溶剂条件下的KAI（SO4）2-12H2O（明矾）催化一锅三组分合成2-烷基和2-芳基-4（3H）-喹唑啉酮
2. KAI（SO4）2-12H2O （Alum） Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4（3H）-quinazolinone under Microwave Irradiation and Solvent Free Conditions [J] . Mohammadi Ali A., Sadat Hossini S. S.t 中国化学：英文版 . 2011,第009期

机译：微波辐射和无溶剂条件下的KAI（SO4）2-12H2O（明矾）催化一锅三组分合成2-烷基和2-芳基-4（3H）-喹唑啉酮
3. One-pot solvent-free synthesis of 2, 3-disubstituted 4(3H)- quinazolinones catalyzed by long-chain double SO3H-functionalized Bronsted acidic ionic liquids under microwave irradiation [J] . Li Xinzhong, Lin Qi, Wang Lefu Journal of the Iranian Chemical Society . 2015,第5期

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机译：Yb（OTF）3催化的喹唑啉-4（3H）的一锅合成来自瓦斯酸，胺和邻酯（或甲酸）在无溶剂条件下

KAl(SO4)2·12H2O (Alum) Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4(3H)-quinazolinone under Microwave Irradiation and Solvent Free Conditions

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KAl(SO₄)₂·12H₂O (Alum) Catalyzed One-Pot Three-Component Synthesis of 2-Alkyl and 2-Aryl-4(3H)-quinazolinone under Microwave Irradiation and Solvent Free Conditions