Synthesis and Crystal Structure of 5-N-i-Propyl-2-(2'-nitrobenzenesulfonyl)-glutamine

摘要

The title compound,5-N-i-propyl-2-(2'-nitrobenzenesulfonyl)-glutamine,was synthesized and its structure was confirmed by IR,MS,~1H NMR,and elemental analysis.The single crystal structure of the title compound was determined by X-ray diffraction.The crystal belongs to Monoclinic,space group P2(1),with a=0.69281(11)nm,b=0.76508(12),c=1.5843(3)nm,alpha=90 deg,beta=90.941(3)deg,gamma=90 deg,V=0.8397(2)nm~3,Z=2,D_c=1.477 g/cm~3 mu=0.236 mm~(-1),F(000)=392,R=0.0297,and wR=0.0664.