A structurally-characterized NbCl_5-NHC adduct

Marco Bortoluzzi; Eleonora Ferretti; Fabio Marchetti; Guido Pampaloni; Stefano Zacchini

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A structurally-characterized NbCl_5-NHC adduct

机译：NbCl_5-NHC加合物的结构表征

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摘要

The selective reactions of niobium pentachloride with two bulky NHC carbenes afforded NbCl_5(NHC) complexes, bearing the highest oxidation state ever found for a metal centre in a transition metal halide-NHC adduct. The X-ray structure of 2a is the first one reported fora monodentate NHC-niobium species, and exhibits an abnormally long Nb-C bond.

机译：五氯化铌与两种大体积的NHC卡宾的选择性反应提供了NbCl_5（NHC）配合物，具有过渡金属卤化物-NHC加合物中金属中心所发现的最高氧化态。 2a的X射线结构是单齿NHC-铌物种的第一个报道，并且显示出异常长的Nb-C键。

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《Chemical Communications》 |2014年第34期|4472-4474|共3页
作者
Marco Bortoluzzi; Eleonora Ferretti; Fabio Marchetti; Guido Pampaloni; Stefano Zacchini;
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Ca' Foscari University of Venice, Dipartimento di Scienze Molecolari e Nanosistemi, Dorsoduro 2137,Ⅰ-30123 Venezia, Italy;

University of Pisa, Dipartimento di Chimica e Chimica Industriale, Via Risorgimento 35,Ⅰ-56126 Pisa, Italy;

University of Pisa, Dipartimento di Chimica e Chimica Industriale, Via Risorgimento 35,Ⅰ-56126 Pisa, Italy;

University of Pisa, Dipartimento di Chimica e Chimica Industriale, Via Risorgimento 35,Ⅰ-56126 Pisa, Italy;

University of Bologna, Dipartimento di Chimica Industriale 'Toso Montanari', Viale Risorgimento 4, Ⅰ-40136 Bologna, Italy;

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A structurally-characterized NbCl_5-NHC adduct

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