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Mechanical properties and wear and corrosion resistance of electrodeposited Ni-Co/SiC nanocomposite coating

机译:电沉积Ni-Co / SiC纳米复合镀层的力学性能,耐磨性和耐蚀性

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Ni-Co/SiC nanocomposite coatings with various contents of SiC nano-particulates were prepared by electrodeposition in a Ni-Co plating bath containing SiC nano-particulates to be co-deposited. The influences of the nanoparticulates concentration, current density, stirring rate and temperature of the plating bath on the composition of the coatings were investigated. The shape and size of the SiC nano-particulates were observed and determined using a transmission electron microscope. The polarization behavior of the composite plating bath was examined oil a PAR-273A potentiostat/galvanostat device. The wear behavior of the Ni-Co/SiC nanocomposite coatings was evaluated on a ball-on-disk UMT-2MT test rig. The worn surface morphologies of the Ni-Co/SiC nanocomposite coatings were observed using a scanning electron microscope. The corrosion behavior of the nanocomposite coatings was evaluated by charting the Tafel Curves of the solution of 0.5 mol L-1 NaCl at room temperature. It was found that the cathodic polarization potential of the composite electrolyte increased with increasing SiC concentration in the plating bath. The microhardness and wear and corrosion resistance of the nanocomposite coatings also increased with increasing content of the nano-SiC in the plating bath, and the morphologies of the nanocomposite coatings varied with varying SiC concentration in the plating bath as well. Moreover, the co-deposited SiC nano-particulates were uniformly distributed in the Ni-Co matrix and contributed to greatly increase the microhardness and wear resistance of the Ni-Co alloy coating. (c) 2005 Elsevier B.V. All rights reserved.
机译:通过在包含要共沉积的SiC纳米颗粒的Ni-Co镀浴中进行电沉积,制备具有各种SiC纳米颗粒含量的Ni-Co / SiC纳米复合涂层。研究了纳米粒子的浓度,电流密度,搅拌速度和镀浴温度对涂层组成的影响。使用透射电子显微镜观察并确定SiC纳米颗粒的形状和尺寸。使用PAR-273A恒电位仪/恒电流仪设备检查了复合镀浴的极化行为。 Ni-Co / SiC纳米复合涂层的磨损性能在UMT-2MT球盘试验台上进行了评估。使用扫描电子显微镜观察Ni-Co / SiC纳米复合涂层的磨损表面形态。通过绘制室温下0.5 mol L-1 NaCl溶液的Tafel曲线来评估纳米复合涂层的腐蚀行为。已经发现,随着电镀浴中SiC浓度的增加,复合电解质的阴极极化电位增加。随着镀浴中纳米SiC含量的增加,纳米复合涂层的显微硬度,耐磨性和耐腐蚀性也增加,并且纳米复合涂层的形貌也随着镀浴中SiC浓度的变化而变化。此外,共沉积的SiC纳米颗粒均匀地分布在Ni-Co基体中,并有助于大大提高Ni-Co合金涂层的显微硬度和耐磨性。 (c)2005 Elsevier B.V.保留所有权利。

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