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Facile Facile and green synthesis of highly stable L-cysteine functionalized copper nanoparticles

机译:轻松,绿色合成高度稳定的L-半胱氨酸官能化铜纳米颗粒

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摘要

A simple eco-friendly method for L-cysteine capped copper nanoparticles (CCNPs) synthesis in aqueous solution has been developed. Glucose and L-cysteine were used as reducing agent and capping/functionalizing agent, respectively. Different parameters such as capping agent concentration, pH, reaction temperature, and reducing agent concentration were optimized during the synthesis. The L-cysteine capped copper nanoparticle were characterized by ultraviolet-visible spectroscopy, Fourier transform infrared spectroscopy, X-ray diffraction, Particle size and zeta potential analyser, and high resolution transmission electron microscopy. Spherical shaped cysteine functionalized/capped copper nanoparticles with an average size of 40 nm were found to be highly stable at room temperature (RT) for a period of 1 month (C) 2016 Elsevier B.V. All rights reserved.
机译:已经开发了一种简单的环保方法,用于在水溶液中合成L-半胱氨酸帽的铜纳米粒子(CCNP)。葡萄糖和L-半胱氨酸分别用作还原剂和封端/官能化剂。在合成过程中优化了不同的参数,例如封端剂浓度,pH,反应温度和还原剂浓度。通过紫外-可见光谱,傅里叶变换红外光谱,X射线衍射,粒度和ζ电势分析仪以及高分辨率透射电子显微镜对L-半胱氨酸覆盖的铜纳米粒子进行了表征。发现平均大小为40 nm的球形半胱氨酸官能化/加帽的铜纳米颗粒在室温(RT)下高度稳定1个月(C)2016 Elsevier B.V.保留所有权利。

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