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Effect of Glass Fibers Thermal Treatment on the Mechanical and Thermal Behavior of Polysulfone Based Composites

机译:玻璃纤维热处理对聚砜基复合材料力学和热性能的影响

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摘要

The effect of thermal treatment of glass fibers (GF) on the mechanical and thermo-mechanical properties of polysulfone (PSU) based composites reinforced with GF was investigated. Flexural and shear tests were used to study the composites’ mechanical properties. A dynamic mechanical analysis (DMA) and a heat deflection temperature (HDT) test were used to study the thermo-mechanical properties of composites. The chemical structure of the composites was studied using IR-spectroscopy, and scanning electron microscopy (SEM) was used to illustrate the microstructure of the fracture surface. Three fiber to polymer ratios of initial and preheated GF composites (50/50, 60/40, 70/30 (wt.%)) were studied. The results showed that the mechanical and thermo-mechanical properties improved with an increase in the fiber to polymer ratio. The interfacial adhesion in the preheated composites enhanced as a result of removing the sizing coating during the thermal treatment of GF, which improved the properties of the preheated composites compared with the composites reinforced with initial untreated fibers. The SEM images showed a good distribution of the polymer on the GF surface in the preheated GF composites.
机译:研究了玻璃纤维(GF)的热处理对以GF增强的聚砜(PSU)基复合材料的机械和热机械性能的影响。弯曲和剪切试验用于研究复合材料的机械性能。使用动态力学分析(DMA)和热变形温度(HDT)测试来研究复合材料的热机械性能。使用红外光谱研究了复合材料的化学结构,并使用扫描电子显微镜(SEM)来显示断裂表面的微观结构。研究了初始和预热的GF复合材料的三种纤维与聚合物的比率(50 / 50、60 / 40、70 / 30(wt。%))。结果表明,随着纤维与聚合物比的增加,机械性能和热机械性能得到改善。由于在GF的热处理过程中去除了上浆涂层,预热复合材料中的界面粘合性得到了增强,与使用初始未经处理的纤维增强的复合材料相比,预热复合材料的性能得到了改善。 SEM图像显示了在预热的GF复合材料中聚合物在GF表面上的良好分布。

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