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Optimization of microwave assisted extraction (MAE) and soxhlet extraction of phenolic compound from licorice root

机译:甘草根中微波辅助提取和索氏提取酚类化合物的优化

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摘要

In present study, response surface methodology was used to optimize extraction condition of phenolic compounds from licorice root by microwave application. Investigated factors were solvent (ethanol 80 %, methanol 80 % and water), liquid/solid ratio (10:1–25:1) and time (2–6 min). Experiments were designed according to the central composite rotatable design. The results showed that extraction conditions had significant effect on the extraction yield of phenolic compounds and antioxidant capacities. Optimal condition in microwave assisted method were ethanol 80 % as solvent, extraction time of 5–6 min and liquid/solid ratio of 12.7/1. Results were compared with those obtained by soxhlet extraction. In soxhlet extraction, Optimum conditions were extraction time of 6 h for ethanol 80 % as solvent. Value of phenolic compounds and extraction yield of licorice root in microwave assisted (MAE), and soxhlet were 47.47 mg/g and 16.38 %, 41.709 mg/g and 14.49 %, respectively. These results implied that MAE was more efficient extracting method than soxhlet.
机译:在本研究中,响应面法被用于优化微波条件下从甘草根中提取酚类化合物的条件。研究的因素是溶剂(80%的乙醇,80%的甲醇和水),液/固比(10:1–25:1)和时间(2–6分钟)。根据中央复合旋转设计设计了实验。结果表明,提取条件对酚类化合物的提取得率和抗氧化能力有显着影响。微波辅助法的最佳条件是80%乙醇为溶剂,萃取时间为5-6min,液/固比为12.7 / 1。将结果与通过索氏提取获得的结果进行比较。在索氏提取中,最佳条件是以80%乙醇为溶剂的提取时间为6小时。微波辅助(MAE)和索氏提取物中的酚类化合物和甘草根的提取率分别为47.47 mg / g和16.38%,41.709 mg / g和14.49%。这些结果暗示MAE比索氏提取法更有效。

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