The solid phase microextraction gas chromatography-mass spectrometry (SPME/GC/MS) analytical technique has been used to study quantitatively the outgases from materials aging. The detective method and its conditions have been discussed. The effect of extracting time on analysis results and the linear correlations between the concentration and its peak areas and the repeatability of this method have been researched.. The correlative factors of quantitatively extracting some organic components have been received.
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