首页> 中文期刊> 《航空材料学报》 >FGH4096合金的动态再结晶与晶粒细化研究

FGH4096合金的动态再结晶与晶粒细化研究

             

摘要

Isothermal compression of HIPed (Hot Isostatic Pressed) FGH4096 superalloy in the temperature range 1080 ~ 1140℃ and strain rate range 0.02 ~ ls -1 with deformation from 15% to 50% have been conducted on Gleeble-1500D simulator, Recrystallization nucleation and microstructure evolution during the hot deformation have been revealed by TEM (transmission electron microscopy) and MO( metallographie observation). When compressed with the deformation of 35% or blow, a not fully recrystallized mierostrueture called "Link" microstructure received. Fully recrystallized microstructure obtained when the deformation reached 50%, grain size of which grows as the temperature rise and strain rate decrease. Primary recrystallization nucleation sites could be summarized as follows:PPB (Previous Particle Boundaries), grain boundaries of the recrystallized grain and twin sourse. A fine structure with average 8rainsize of 4p, m obtained by the effect of multiaxial hot deformation as a result.%使用Gleeble-1500D热模拟试验机对热等静压态FGH4096合金进行变形温度1080~1140℃,应变速率0.02~1s-1,变形量15%,35%和50%的等温压缩实验.通过观察微观组织,分析了粉末高温合金动态再结晶的组织演化规律,并通过透射电镜研究了再结晶的形核位置.当变形量在35%及以下时,得到不完全再结晶组织,即"项链"组织;当变形量大于50%时,得到完全的动态再结晶组织.动态再结晶晶粒尺寸随变形温度的升高和应变速率的降低而增大.再结晶形核主要在以下三个位置,即原始颗粒边界,再结晶晶粒边界以及孪晶源.最后利用多方向热变形对晶粒的破碎和细化,得到平均品粒尺寸为4μm的细晶坯料.

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