三嗪类环蕃的合成与表征

摘要

以三聚氯氰、乙胺、二甲胺、甲胺、苯酚、二(4-氨基苯基)甲烷等为原料,经取代、傅克反应和成环反应,合成了一类新型三嗪类杂环蕃(4a,4b,4c),并通过1H NMR、IR和MALDI-TOF-MS对其结构进行了表征.%Some novel heterocyclophanes containing 1,3,5-triazine (4a,4b,4c) were synthesized from cyanuric chloride, ethylamine, dimethylatnine, aniline, phenol and di(4-aminophenyl) methane by substitution , Friedel-Crafts alkylation and cyclization. The structures were characterized by 1H NMR, IR and MALDI-TOF-MS methods.