首页> 外文会议>The Twenty-third annual meeting of the American Society of Precision Engineering and the Twelfth ICPE >DEVELOPMENT OF THE PRIMARY NANOPARTICLE MEASUREMENT STANDARD BY THE ELECTRO-GRAVITATIONAL AEROSOL BALANCE
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DEVELOPMENT OF THE PRIMARY NANOPARTICLE MEASUREMENT STANDARD BY THE ELECTRO-GRAVITATIONAL AEROSOL BALANCE

机译:重力气溶胶平衡法开发主要的纳米颗粒测量标准

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摘要

In order to achieve higher accuracy and lower uncertainty for nanoparticle size measurement, the electro-gravitational aerosol balance method has been used to develop the primary nanoparticle size standard system at Center for Measurement Standards, because of the simplicity of its principle. The measurements for the particle sizes ranging from 100 nm to 500 nm are currently in progress.rnBecause of the different measurement principles applied in these techniques for nanoparticle size characterizations, the obtained measurement results do not always agree with each other. In some cases, the deviation on the measurements of the same sample is rather significant that would easily lead to the questions of which instrument could be trusted when it comes to determining the sizes of certain nanoparticles and how to translate the difference in measurements among these instruments. Certainly, there are number reasons that would attribute to the disagreement in measurements.rnIt would definitely improve measurement consistency and accuracy if there exist particulate reference standards, international or industrial standards that would sufficiently comprehend details of the measurements. Additionally, measurement consistency and accuracy could be improved, if the nanoscale instruments in the laboratories can be properly evaluated with uncertainty budget, and validated with recognized protocols.
机译:为了获得更高的精度和更低的纳米粒度测量不确定度,由于其原理的简单性,电引力气溶胶平衡法已被用于在测量标准中心开发主要的纳米粒度标准体系。目前正在对100 nm至500 nm的粒径进行测量。由于在这些技术中对纳米粒径表征使用了不同的测量原理,因此获得的测量结果并不总是彼此一致的。在某些情况下,同一样品的测量值上的偏差相当大,这很容易引起问题,即在确定某些纳米颗粒的尺寸以及如何转换这些仪器之间的测量差异时,可以信任哪种仪器。当然,有许多原因可归因于测量的分歧。如果存在能够充分理解测量细节的微粒参考标准,国际或工业标准,它将绝对提高测量的一致性和准确性。此外,如果实验室中的纳米仪器可以用不确定性预算进行适当评估,并通过公认的协议进行验证,则可以提高测量的一致性和准确性。

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