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Nanoindentation and nanowear studies of thin carbon coatings

机译:薄碳涂层的纳米压痕和纳米磨损研究

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Thin film magnetic disks and head-slideers require protective overcoats, usually some form of carbon, to guard the magnetic elements against corrosion and wear and to provide long interface durability. The mechanical properties of these coatings are important for assessing their tribological performance. In this paper we present the results of nanomechanical properties of amorphous carbon (a-C) and nitrogenated carbon (a-C) and nitrogenated carbon (CN) films deposited on Si(100). a-C and CN films were deposited on silicon by Facing Target Sputtering (FTS) technique. The elemental composition and bond characterization of a-C and CN films have been determined by X-ray Photoelectron spectroscopy (XPS). Nanoindentation experiments were performed using Hysitron Triboscope~(circle R) in the load range of 10-200 mu n, using a sharp 90 deg 3-sided pyramidal diamond tip (50+-10 nm radius). Hardness and Young's modulus of elasticity were determined from the load-displacement data. Nanowear studies were performed on the 10 and 20 nm a-C and CN films to determine the critical load. Below the critical load no significant wear is observed. Above the critical load however, the wear increases sharply. Abrasive wear seems to be the cause of the sharp increase in wear depth in case of a-C film. From the above observation, CN films exhibit excellent mechanical properties owing to its superior hardness property.
机译:薄膜磁盘和磁头滑块需要保护层,通常是某种形式的碳,以保护磁性元件免受腐蚀和磨损并提供长久的界面耐久性。这些涂层的机械性能对于评估其摩擦性能很重要。在本文中,我们介绍了沉积在Si(100)上的非晶碳(a-C)和氮化碳(a-C)和氮化碳(CN)薄膜的纳米力学性能。通过面对靶溅射(FTS)技术将a-C和CN膜沉积在硅上。 a-C和CN膜的元素组成和键表征已通过X射线光电子能谱(XPS)确定。纳米压痕实验是使用Hysitron Triboscope?(圆圈R)在10-200μn的负载范围内进行的,使用的是尖锐的90度3边金字塔形钻石尖端(半径为50 + -10 nm)。硬度和杨氏弹性模量由载荷-位移数据确定。在10和20 nm的a-C和CN膜上进行了纳米磨损研究,以确定临界载荷。在临界载荷以下,没有观察到明显的磨损。但是,超过临界负荷,磨损会急剧增加。对于a-C膜,磨料磨损似乎是磨损深度急剧增加的原因。由以上观察可知,CN膜由于具有优异的硬度,因此具有优异的机械性能。

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